4',7'-O-benzylidene derivative of methyl 2,3,6-tri-O-acetyl-4-deoxy-4-<(1S)-(1,2,4/3,5,6)-2,3,6-triacetoxy-4-hydroxy-5-hydroxymethyl-1-cyclohexylamino>-α-D-glucopyranoside

Base Information

Chemical Name:4',7'-O-benzylidene derivative of methyl 2,3,6-tri-O-acetyl-4-deoxy-4-<(1S)-(1,2,4/3,5,6)-2,3,6-triacetoxy-4-hydroxy-5-hydroxymethyl-1-cyclohexylamino>-α-D-glucopyranoside
CAS No.:84659-10-9
Molecular Formula:C₃₃H₄₃NO₁₆
Molecular Weight:709.702
Hs Code.:

4',7'-O-benzylidene derivative of methyl 2,3,6-tri-O-acetyl-4-deoxy-4-<(1S)-(1,2,4/3,5,6)-2,3,6-triacetoxy-4-hydroxy-5-hydroxymethyl-1-cyclohexylamino>-α-D-glucopyranoside

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Chemical Property of 4',7'-O-benzylidene derivative of methyl 2,3,6-tri-O-acetyl-4-deoxy-4-<(1S)-(1,2,4/3,5,6)-2,3,6-triacetoxy-4-hydroxy-5-hydroxymethyl-1-cyclohexylamino>-α-D-glucopyranoside

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Technology Process of 4',7'-O-benzylidene derivative of methyl 2,3,6-tri-O-acetyl-4-deoxy-4-<(1S)-(1,2,4/3,5,6)-2,3,6-triacetoxy-4-hydroxy-5-hydroxymethyl-1-cyclohexylamino>-α-D-glucopyranoside

There total 13 articles about 4',7'-O-benzylidene derivative of methyl 2,3,6-tri-O-acetyl-4-deoxy-4-<(1S)-(1,2,4/3,5,6)-2,3,6-triacetoxy-4-hydroxy-5-hydroxymethyl-1-cyclohexylamino>-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4181-01-5
Methyl 4-Azido-4-deoxy-α-D-glucopyranoside

: 84659-10-9,84710-63-4,101758-37-6
Acetic acid (4aS,5R,6S,7S,8S,8aR)-7,8-diacetoxy-6-((2S,3R,4S,5R,6S)-4,5-diacetoxy-2-acetoxymethyl-6-methoxy-tetrahydro-pyran-3-ylamino)-2-phenyl-hexahydro-benzo[1,3]dioxin-5-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / H₂ / Raney nickel / methanol

2: 2.) pyridine / 1.) i-PrOH, 120 deg C, 117 h; 2.) r.t.

With pyridine; hydrogen; nickel; In methanol;
DOI:10.1246/cl.1982.1729

Reference yield:

: 4181-01-5
Methyl 4-Azido-4-deoxy-α-D-glucopyranoside

: 84659-10-9,84710-63-4,101758-37-6
Acetic acid (4aR,5S,6R,7R,8R,8aS)-7,8-diacetoxy-6-((2S,3R,4S,5R,6S)-4,5-diacetoxy-2-acetoxymethyl-6-methoxy-tetrahydro-pyran-3-ylamino)-2-phenyl-hexahydro-benzo[1,3]dioxin-5-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / H₂ / Raney nickel / methanol

2: 2.) pyridine / 1.) i-PrOH, 120 deg C, 117 h; 2.) r.t.

With pyridine; hydrogen; nickel; In methanol;
DOI:10.1246/cl.1982.1729

Reference yield:

: 4181-01-5
Methyl 4-Azido-4-deoxy-α-D-glucopyranoside

: 84659-10-9,84710-63-4,101758-37-6
Acetic acid (2S,4aR,5S,6R,7R,8R,8aS)-7,8-diacetoxy-6-((2S,3R,4S,5R,6S)-4,5-diacetoxy-2-acetoxymethyl-6-methoxy-tetrahydro-pyran-3-ylamino)-2-phenyl-hexahydro-benzo[1,3]dioxin-5-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / H₂ / Raney nickel T-4 / methanol / 2500.7 Torr / Ambient temperature

2: 1.) 2-propanol, 120 deg C, 117 h, 2.) pyridine, room temp., overnight

With hydrogen; Raney nickel T-4; In methanol;
DOI:10.1016/0008-6215(85)85016-3