β-[(2-ethoxycarbonyl-ethyl)-benzoyl-amino]-isovaleric acid ethyl ester

Base Information

Chemical Name:β-[(2-ethoxycarbonyl-ethyl)-benzoyl-amino]-isovaleric acid ethyl ester
CAS No.:856989-94-1
Molecular Formula:C₁₉H₂₇NO₅
Molecular Weight:349.427
Hs Code.:

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Chemical Property of β-[(2-ethoxycarbonyl-ethyl)-benzoyl-amino]-isovaleric acid ethyl ester

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Technology Process of β-[(2-ethoxycarbonyl-ethyl)-benzoyl-amino]-isovaleric acid ethyl ester

There total 2 articles about β-[(2-ethoxycarbonyl-ethyl)-benzoyl-amino]-isovaleric acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85532-42-9
ethyl 3-amino-3-methylbutanoate

: 856989-94-1
β-[(2-ethoxycarbonyl-ethyl)-benzoyl-amino]-isovaleric acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid

2: triethylamine; benzene

With acetic acid; triethylamine; benzene;

Reference yield:

: 140-88-5,9003-32-1
ethyl acrylate

: 856989-94-1
β-[(2-ethoxycarbonyl-ethyl)-benzoyl-amino]-isovaleric acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid

2: triethylamine; benzene

With acetic acid; triethylamine; benzene;

Reference yield:

: 856989-94-1
β-[(2-ethoxycarbonyl-ethyl)-benzoyl-amino]-isovaleric acid ethyl ester

: 104094-98-6
(+/-)-(2,2-dimethyl-[4]piperidyl)-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: sodium; benzene; ethanol

2: water; KOH-solution

3: benzene; ammonium acetate; acetic acid / Abtrennen des entstehenden H₂O

4: platinum; dioxane / Hydrogenation

5: aqueous KOH / 140 - 150 °C / Erhitzen des Reaktionsprodukts auf 200grad und Erwaermen der danach erhaltenen Essigsaeure mit aethanol. HCl

With 1,4-dioxane; ammonium acetate; potassium hydroxide; ethanol; water; sodium; acetic acid; platinum; benzene;