Picric acid; compound with 6-chloro-1,2,3,4-tetrahydro-isoquinoline

Base Information

Chemical Name:Picric acid; compound with 6-chloro-1,2,3,4-tetrahydro-isoquinoline
CAS No.:33537-98-3
Molecular Formula:C₆H₃N₃O₇*C₉H₁₀ClN
Molecular Weight:396.744
Hs Code.:

Synonyms:

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Chemical Property of Picric acid; compound with 6-chloro-1,2,3,4-tetrahydro-isoquinoline

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Technology Process of Picric acid; compound with 6-chloro-1,2,3,4-tetrahydro-isoquinoline

There total 5 articles about Picric acid; compound with 6-chloro-1,2,3,4-tetrahydro-isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1529-41-5
3-chloro-benzeneacetonitrile

: 33537-98-3
Picric acid; compound with 6-chloro-1,2,3,4-tetrahydro-isoquinoline

Guidance literature:: Multi-step reaction with 6 steps

1: NaBH₄, SnCl₄

2: 77 percent / potassium carbonate / H₂O; toluene; benzene / 1.) 0 deg C, 30 min; 2.) 35 deg C, 24 h

3: methanesulphonic acid / acetic anhydride; 1,2-dichloro-ethane / 35 °C

4: 67 percent / methanesulphonic acid / acetic anhydride; 1,2-dichloro-ethane / 35 °C

5: aqueous HCl / 2-methyl-propan-2-ol / 10 h / 75 °C

With hydrogenchloride; sodium tetrahydroborate; methanesulfonic acid; tin(IV) chloride; potassium carbonate; In water; acetic anhydride; 1,2-dichloro-ethane; toluene; tert-butyl alcohol; benzene;

Reference yield:

: 111874-98-7
3-[2-(3-Chloro-phenyl)-ethylsulfamoyl]-propionic acid methyl ester

: 33537-98-3
Picric acid; compound with 6-chloro-1,2,3,4-tetrahydro-isoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: methanesulphonic acid / acetic anhydride; 1,2-dichloro-ethane / 35 °C

2: 67 percent / methanesulphonic acid / acetic anhydride; 1,2-dichloro-ethane / 35 °C

3: aqueous HCl / 2-methyl-propan-2-ol / 10 h / 75 °C

With hydrogenchloride; methanesulfonic acid; In acetic anhydride; 1,2-dichloro-ethane; tert-butyl alcohol;

Reference yield:

: 111875-08-2
N-(2-methoxycarbonylethylsulfonyl)-6-chloro-1,2,3,4-tetrahydroisoquinoline

: 33537-98-3
Picric acid; compound with 6-chloro-1,2,3,4-tetrahydro-isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: aqueous HCl / 2-methyl-propan-2-ol / 10 h / 75 °C

With hydrogenchloride; In tert-butyl alcohol;