C₁₈H₂₆INO₃S

Base Information

• Chemical Name: C₁₈H₂₆INO₃S
• CAS No.: 1350810-25-1
• Molecular Formula: C₁₈H₂₆INO₃S
• Molecular Weight: 463.38
• Mol file: 1350810-25-1.mol

Synonyms:

Chemical Property of C₁₈H₂₆INO₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₂₆INO₃S

There total 4 articles about C₁₈H₂₆INO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H36INO4S (1350810-19-3) → C18H26INO3S (1350810-25-1)

Guidance literature:

With water; toluene-4-sulfonic acid; In acetone; at 80 ℃;

DOI:10.1039/c1cc15257b

Reference yield:

C16H24INO2S → C18H26INO3S (1350810-25-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetone / Reflux

2: water; toluene-4-sulfonic acid / acetone / 80 °C

With water; potassium carbonate; toluene-4-sulfonic acid; In acetone;

DOI:10.1039/c1cc15257b

Reference yield:

C9H17IO (148457-52-7) → C18H26INO3S (1350810-25-1)

Guidance literature:

Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C

2: potassium carbonate / acetone / Reflux

3: water; toluene-4-sulfonic acid / acetone / 80 °C

With di-isopropyl azodicarboxylate; water; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; acetone; 1: Mitsunobu reaction;

DOI:10.1039/c1cc15257b

upstream raw materials:

C₉H₁₇IO

C₂₂H₃₆INO₄S

hep-2-yn-1-ol

Downstream raw materials:

C₁₉H₂₈N₂O₃S

C₁₈H₂₅NO₃S

C₁₉H₂₉IN₂O₃S