(C₅H₄NC(C₆H₅)NNCO)2C₅H₂NClNi

Base Information

• Chemical Name: (C₅H₄NC(C₆H₅)NNCO)2C₅H₂NClNi
• CAS No.: 855005-63-9
• Molecular Formula: C₃₁H₂₀ClN₇NiO₂
• Molecular Weight: 616.688
• Mol file: 855005-63-9.mol

Synonyms:

Chemical Property of (C₅H₄NC(C₆H₅)NNCO)2C₅H₂NClNi

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (C₅H₄NC(C₆H₅)NNCO)2C₅H₂NClNi

There total 1 articles about (C₅H₄NC(C₆H₅)NNCO)2C₅H₂NClNi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

nickel(II) carbonate (719261-06-0) + C5H4NCOHN2CCH3CNOHCH3 (111073-23-5) → (C5H4NC(C6H5)NNCO)2C5H2NClNi (855005-63-9)

Guidance literature:

In ethanol; acetonitrile; NiCO3 suspd. in 1:1 MeCN/EtOH; organic ligand added; mixt. heated; wateradded; heating continued for 15 min; filtered; allowed to stand at room temp. for 2 days; elem. anal.;

DOI:10.1016/j.poly.2005.02.016

Reference yield: 50.0%

copper(II) nitrate trihydrate + (C5H4NC(C6H5)NNCO)2C5H2NClNi (855005-63-9) → Cu3(C5H4NC(C6H5)NNC(O)C5H2NClCOO)2(H2O)4(2+)*2NO3(1-)*4H2O=Cu3(C5H4NC(C6H5)NNC(O)C5H2NClCOO)2(H2O)4(NO3)2*4H2O

Guidance literature:

In methanol; chloroform; addn. of methanolic soln. of Cu(NO3)2*3H2O to a soln. of Ni complex in CHCl3, warming for 45 min; elem. anal.;

DOI:10.1039/b618067a

upstream raw materials:

nickel(II) carbonate

C₅H₄NCOHN₂CCH₃CNOHCH₃