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Selenolo[2,3-b][1]benzothiophene

Base Information Edit
  • Chemical Name:Selenolo[2,3-b][1]benzothiophene
  • CAS No.:40197-95-3
  • Molecular Formula:C10H6SSe
  • Molecular Weight:237.184
  • Hs Code.:
  • Mol file:40197-95-3.mol
Selenolo[2,3-b][1]benzothiophene

Synonyms:

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of Selenolo[2,3-b][1]benzothiophene Edit
Chemical Property:
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Technology Process of Selenolo[2,3-b][1]benzothiophene

There total 4 articles about Selenolo[2,3-b][1]benzothiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With copper; In quinoline; for 4h; Reflux;
DOI:10.1002/chem.201903958
Guidance literature:
Multi-step reaction with 3 steps
1.1: selenium; sodium tetrahydroborate; sodium hydride / tetrahydrofuran; ethanol / 2 h / 0 - 20 °C / Inert atmosphere
1.2: 1 h / Inert atmosphere
1.3: 12 h / 20 °C / Inert atmosphere
2.1: sodium hydroxide / methanol; water / 6 h / Reflux
3.1: copper / quinoline / 4 h / Reflux
With selenium; sodium tetrahydroborate; copper; sodium hydride; sodium hydroxide; In tetrahydrofuran; quinoline; methanol; ethanol; water;
DOI:10.1002/chem.201903958
Guidance literature:
Multi-step reaction with 2 steps
1: sodium hydroxide / methanol; water / 6 h / Reflux
2: copper / quinoline / 4 h / Reflux
With copper; sodium hydroxide; In quinoline; methanol; water;
DOI:10.1002/chem.201903958
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