(S)-5⁶,7^{6,7_{,96-tetramethoxy-72-methyl-7}1,2,3,4}-tetrahydro-4,8-dioxa-12-aza-3(1,4),5,9(1,3)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-methyl ester

Base Information

• Chemical Name: (S)-5⁶,7^{6,7_{,96-tetramethoxy-72-methyl-7}1,2,3,4}-tetrahydro-4,8-dioxa-12-aza-3(1,4),5,9(1,3)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-methyl ester
• CAS No.: 36455-03-5
• Molecular Formula: C₄₃H₅₂N₂O₁₀
• Molecular Weight: 756.893

Synonyms:

Chemical Property of (S)-5⁶,7^{6,7_{,96-tetramethoxy-72-methyl-7}1,2,3,4}-tetrahydro-4,8-dioxa-12-aza-3(1,4),5,9(1,3)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (S)-5⁶,7^{6,7_{,96-tetramethoxy-72-methyl-7}1,2,3,4}-tetrahydro-4,8-dioxa-12-aza-3(1,4),5,9(1,3)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-methyl ester

There total 1 articles about (S)-5⁶,7^{6,7_{,96-tetramethoxy-72-methyl-7}1,2,3,4}-tetrahydro-4,8-dioxa-12-aza-3(1,4),5,9(1,3)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ (S)-56,76,7,96-tetramethoxy-72-methyl-71,2,3,4-tetrahydro-4,8-dioxa-12-aza-3(1,4),5,9(1,3)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-methyl ester (36455-03-5)

Guidance literature:

Phenolbase (40), Methyl-<4-bromphenylacetat> (41);

Reference yield:

(S)-56,76,7,96-tetramethoxy-72-methyl-71,2,3,4-tetrahydro-4,8-dioxa-12-aza-3(1,4),5,9(1,3)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-methyl ester (36455-03-5) → (+)-O-methylthalicberine (5096-71-9,25161-55-1)

Guidance literature:

Multi-step reaction with 4 steps

1: (i) aq. NaOH, MeOH, (ii) 4-nitro-phenol, DCC, AcOEt, Et₂O, (iii) CF₃CO₂H, (iv) Py, DMF

2: POCl₃ / CHCl₃

3: NaBH₄ / methanol

4: (i) MeOH, (ii) NaBH₄

With sodium tetrahydroborate; trichlorophosphate; In methanol; chloroform;

Reference yield:

(S)-56,76,7,96-tetramethoxy-72-methyl-71,2,3,4-tetrahydro-4,8-dioxa-12-aza-3(1,4),5,9(1,3)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-methyl ester (36455-03-5) → 6,7,12,7'-tetramethoxy-2-methyl-thalicber-1'-ene (5979-99-7)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) aq. NaOH, MeOH, (ii) 4-nitro-phenol, DCC, AcOEt, Et₂O, (iii) CF₃CO₂H, (iv) Py, DMF

2: POCl₃ / CHCl₃

With trichlorophosphate; In chloroform;

Downstream raw materials:

6,7,12,7'-tetramethoxy-2-methyl-thalicber-1'-ene

(+)-O-methylthalicberine

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