8-methoxycarbonyloctyl 2-acetamido-3,6-di-O-benzyloxymethyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:8-methoxycarbonyloctyl 2-acetamido-3,6-di-O-benzyloxymethyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside
CAS No.:84455-81-2
Molecular Formula:C₆₈H₈₀N₂O₁₈
Molecular Weight:1213.39
Hs Code.:

8-methoxycarbonyloctyl 2-acetamido-3,6-di-O-benzyloxymethyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Chemical Property of 8-methoxycarbonyloctyl 2-acetamido-3,6-di-O-benzyloxymethyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Technology Process of 8-methoxycarbonyloctyl 2-acetamido-3,6-di-O-benzyloxymethyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

There total 12 articles about 8-methoxycarbonyloctyl 2-acetamido-3,6-di-O-benzyloxymethyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 84439-22-5
3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-α-D-galactopyranosyl bromide

: 84439-26-9
8-methoxycarbonyloctyl 2-acetamido-3,6-di-O-benzyloxymethyl-2-deoxy-β-D-glucopyranoside

: 84455-81-2
8-methoxycarbonyloctyl 2-acetamido-3,6-di-O-benzyloxymethyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-α-D-galactopyranosyl)-β-D-glucopyranoside

: 84455-81-2
8-methoxycarbonyloctyl 2-acetamido-3,6-di-O-benzyloxymethyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; for 42h; Ambient temperature;
DOI:10.1016/0008-6215(82)84034-2

Reference yield: 36.0%

: 84439-22-5
3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-α-D-galactopyranosyl bromide

: 84439-26-9
8-methoxycarbonyloctyl 2-acetamido-3,6-di-O-benzyloxymethyl-2-deoxy-β-D-glucopyranoside

: 84455-81-2
8-methoxycarbonyloctyl 2-acetamido-3,6-di-O-benzyloxymethyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-α-D-galactopyranosyl)-β-D-glucopyranoside

: 84455-81-2
8-methoxycarbonyloctyl 2-acetamido-3,6-di-O-benzyloxymethyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; for 42h; Ambient temperature;
DOI:10.1016/0008-6215(82)84034-2

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 84455-81-2
8-methoxycarbonyloctyl 2-acetamido-3,6-di-O-benzyloxymethyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-2-O-p-nitrobenzoyl-α-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-lutidine / dimethylformamide / 16 h / Ambient temperature

2: CF₃SO₂OAg / CH₂Cl₂; various solvent(s) / 42 h / Ambient temperature

With 2,6-dimethylpyridine; silver trifluoromethanesulfonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(82)84034-2