Technology Process of C27H34N7O13P3
There total 8 articles about C27H34N7O13P3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tributyl-amine; phosphoric acid; dicyclohexyl-carbodiimide;
In
pyridine;
at 20 ℃;
for 48h;
Inert atmosphere;
DOI:10.1039/c2cc33552b
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: ammonium hydroxide / 1,4-dioxane / 0 - 20 °C / Inert atmosphere
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere
3.1: 1H-tetrazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
3.2: 1.33 h / 0 - 20 °C / Inert atmosphere
4.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere
5.1: tributyl-amine; phosphoric acid; dicyclohexyl-carbodiimide / pyridine / 48 h / 20 °C / Inert atmosphere
With
1H-tetrazole; ammonium hydroxide; tributyl-amine; phosphoric acid; tetrabutyl ammonium fluoride; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
tetrahydrofuran; 1,4-dioxane; pyridine; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc33552b
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1H-tetrazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
1.2: 1.33 h / 0 - 20 °C / Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere
3.1: tributyl-amine; phosphoric acid; dicyclohexyl-carbodiimide / pyridine / 48 h / 20 °C / Inert atmosphere
With
1H-tetrazole; tributyl-amine; phosphoric acid; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
pyridine; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc33552b