N-methyl-2-(methylsulfinyl)-N-acetamide

Base Information

Chemical Name:N-methyl-2-(methylsulfinyl)-N-acetamide
CAS No.:133363-49-2
Molecular Formula:C₁₃H₁₇NO₂S
Molecular Weight:251.349
Hs Code.:

N-methyl-2-(methylsulfinyl)-N-<o-(prop-1-enyl)phenyl>acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-2-(methylsulfinyl)-N-acetamide

Chemical Property:

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Technology Process of N-methyl-2-(methylsulfinyl)-N-acetamide

There total 2 articles about N-methyl-2-(methylsulfinyl)-N-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 133363-45-8,133363-78-7
N-methyl-2-(methylthio)-N-acetamide

: 133363-49-2,133363-50-5
N-methyl-2-(methylsulfinyl)-N-acetamide

Guidance literature:: With sodium periodate; In water; acetone; for 16h; Ambient temperature;
DOI:10.1248/cpb.38.3331

Reference yield:

: 1127329-76-3
N-methyl-o-(prop-1-enyl)aniline

: 133363-49-2,133363-50-5
N-methyl-2-(methylsulfinyl)-N-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / ethyl acetate / 16 h / Ambient temperature

2: 89 percent / NaIO₄ / H₂O; acetone / 16 h / Ambient temperature

With dmap; sodium periodate; dicyclohexyl-carbodiimide; In water; ethyl acetate; acetone;
DOI:10.1248/cpb.38.3331

Reference yield:

: 133363-49-2,133363-50-5
N-methyl-2-(methylsulfinyl)-N-acetamide

: 133363-53-8
4-ethenyl-1-methyl-2(1H)-quinolinone

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / trifluoroacetic anhydride / CH₂Cl₂ / 0.5 h / Ambient temperature; various N--2-(methylsulfinyl)acetamides, other reagent, other conditions

2: NaIO₄ / CH₂Cl₂ / Ambient temperature

3: NaHCO₃ / toluene / 2 h / Heating

With sodium periodate; sodium hydrogencarbonate; trifluoroacetic anhydride; In dichloromethane; toluene;
DOI:10.1248/cpb.38.3331