3-acetyl-3,5,12-trihydroxy-1-[5-hydroxy-4-(4-hydroxyphenylaminocarbonylamino)-6-methylperhydro-2-pyranoloxy]-10-methoxy-(1S,3S)-1,2,3,4,6,11-hexahydro-6,11-naphthacenedione

Base Information

Chemical Name:3-acetyl-3,5,12-trihydroxy-1-[5-hydroxy-4-(4-hydroxyphenylaminocarbonylamino)-6-methylperhydro-2-pyranoloxy]-10-methoxy-(1S,3S)-1,2,3,4,6,11-hexahydro-6,11-naphthacenedione
CAS No.:371754-31-3
Molecular Formula:C₃₆H₃₈N₂O₁₂
Molecular Weight:690.704
Hs Code.:

3-acetyl-3,5,12-trihydroxy-1-[5-hydroxy-4-(4-hydroxyphenylaminocarbonylamino)-6-methylperhydro-2-pyranoloxy]-10-methoxy-(1S,3S)-1,2,3,4,6,11-hexahydro-6,11-naphthacenedione

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Chemical Property of 3-acetyl-3,5,12-trihydroxy-1-[5-hydroxy-4-(4-hydroxyphenylaminocarbonylamino)-6-methylperhydro-2-pyranoloxy]-10-methoxy-(1S,3S)-1,2,3,4,6,11-hexahydro-6,11-naphthacenedione

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Technology Process of 3-acetyl-3,5,12-trihydroxy-1-[5-hydroxy-4-(4-hydroxyphenylaminocarbonylamino)-6-methylperhydro-2-pyranoloxy]-10-methoxy-(1S,3S)-1,2,3,4,6,11-hexahydro-6,11-naphthacenedione

There total 2 articles about 3-acetyl-3,5,12-trihydroxy-1-[5-hydroxy-4-(4-hydroxyphenylaminocarbonylamino)-6-methylperhydro-2-pyranoloxy]-10-methoxy-(1S,3S)-1,2,3,4,6,11-hexahydro-6,11-naphthacenedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 20830-81-3
DNR

: 371754-30-2
4‐nitrophenyl N‐[2‐(4‐hydroxyphenyl)ethyl]carbamate

: 371754-31-3
3-acetyl-3,5,12-trihydroxy-1-[5-hydroxy-4-(4-hydroxyphenylaminocarbonylamino)-6-methylperhydro-2-pyranoloxy]-10-methoxy-(1S,3S)-1,2,3,4,6,11-hexahydro-6,11-naphthacenedione

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 3h;
DOI:10.1016/S0968-0896(01)00039-6

Reference yield:

: 51-67-2
tyrosamine

: 371754-31-3
3-acetyl-3,5,12-trihydroxy-1-[5-hydroxy-4-(4-hydroxyphenylaminocarbonylamino)-6-methylperhydro-2-pyranoloxy]-10-methoxy-(1S,3S)-1,2,3,4,6,11-hexahydro-6,11-naphthacenedione

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / CH₂Cl₂ / 2 h / Heating

2: 46 percent / diisopropylethylamine / dimethylformamide / 3 h

With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(01)00039-6