Os₃(CO)11(C₆H₅)4P₄CH₂

Base Information

Chemical Name:Os₃(CO)11(C₆H₅)4P₄CH₂
CAS No.:445379-72-6
Molecular Formula:C₃₆H₂₂O₁₁Os₃P₄
Molecular Weight:1325.06
Hs Code.:

Os<sub>3</sub>(CO)11(C<sub>6</sub>H<sub>5</sub>)4P<sub>4</sub>CH<sub>2</sub>

Synonyms:

Suppliers and Price of Os₃(CO)11(C₆H₅)4P₄CH₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Os₃(CO)11(C₆H₅)4P₄CH₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Os₃(CO)11(C₆H₅)4P₄CH₂

There total 1 articles about Os₃(CO)11(C₆H₅)4P₄CH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 133869-39-3,65702-94-5
undecacarbonyl(acetonitrile)triosmium

: 40425-94-3,63357-22-2,879280-62-3,879280-63-4,879280-64-5
1,2,3,4-tetraphenylcyclo-5-carba-1,2,3,4-tetraphosphine

: 445379-72-6
Os₃(CO)11(C₆H₅)4P₄CH₂

Guidance literature:: In dichloromethane; the mixt. (1:1) in CH2Cl2 was stirred at room temp. overnight; evapd. to dryness, dissolved in min CH2Cl2, TLC (CH2Cl2-hexane); elem. anal.;
DOI:10.1021/ic025589c

Reference yield: 74.0%

: 445379-72-6
Os₃(CO)11(C₆H₅)4P₄CH₂

: [Os3(CO)10(μ-1,4-η2-(PPh)4CH2)]

Guidance literature:: In toluene; byproducts: CO; a soln. in toluene was heated overnight at a 100°C oil bath; TLC (CH2Cl2-hexane);
DOI:10.1021/ic025589c

Reference yield: 38.0%

: decacarbonyltriosmiumdihydride

: 445379-72-6
Os₃(CO)11(C₆H₅)4P₄CH₂

: [(H2Os3(CO)8)(μ3-1,2,4-η4-(PPh)4CH2)(Os3(CO)11)]

Guidance literature:: In toluene; a soln. in toluene was heated for 4 h at a 100°C oil bath; TLC (CH2Cl2-hexane); elem. anal.;
DOI:10.1021/ic025589c