N-phenyl-3-amino-4-methoxyanthranilic acid

Base Information

Chemical Name:N-phenyl-3-amino-4-methoxyanthranilic acid
CAS No.:106976-19-6
Molecular Formula:C₁₄H₁₄N₂O₃
Molecular Weight:258.277
Hs Code.:

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Chemical Property of N-phenyl-3-amino-4-methoxyanthranilic acid

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Technology Process of N-phenyl-3-amino-4-methoxyanthranilic acid

There total 6 articles about N-phenyl-3-amino-4-methoxyanthranilic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106976-03-8
4-Methoxy-3-nitro-2-phenylamino-benzoic acid

: 106976-19-6
N-phenyl-3-amino-4-methoxyanthranilic acid

Guidance literature:: With sodium tetrahydroborate; sodium methylate; In methanol;
DOI:10.1021/jm00388a017

Reference yield:

: 16554-47-5
3-methoxy-2-nitroaniline

: 106976-19-6
N-phenyl-3-amino-4-methoxyanthranilic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 51 percent / hydroxylamine sulfate, sodium sulfate, water / 8 h / 60 - 80 °C

2: 91 percent / 80percent aq. H₂SO₄ / 0.25 h / 55 - 60 °C

3: 90 percent / 2N NaOH, 27percent aq. H₂O₂ / 0.25 h

4: 1.) conc. H₂SO₄, NaNO₂, 85percent phosphoric acid, 2.) urea, 3.) KI

5: 50 percent / CuCl, Cu, N-ethylmorpholine / various solvent(s) / 15 h / 70 - 80 °C

6: NaBH₄, MeONa / methanol

With N-ethylmorpholine;; sodium hydroxide; sodium tetrahydroborate; phosphoric acid; sulfuric acid; water; dihydrogen peroxide; sodium methylate; copper; hydroxylamine sulfate; sodium sulfate; urea; potassium iodide; copper(l) chloride; sodium nitrite; In methanol;
DOI:10.1021/jm00388a017

Reference yield:

: 106976-18-5
4-methoxy-3-nitroanthranilic acid

: 106976-19-6
N-phenyl-3-amino-4-methoxyanthranilic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) conc. H₂SO₄, NaNO₂, 85percent phosphoric acid, 2.) urea, 3.) KI

2: 50 percent / CuCl, Cu, N-ethylmorpholine / various solvent(s) / 15 h / 70 - 80 °C

3: NaBH₄, MeONa / methanol

With N-ethylmorpholine;; sodium tetrahydroborate; phosphoric acid; sulfuric acid; sodium methylate; copper; urea; potassium iodide; copper(l) chloride; sodium nitrite; In methanol;
DOI:10.1021/jm00388a017