Technology Process of 9-(2,3,5-tri-O-benzoyl-β-L-ribofuranosyl)-N-palmitoylguanosine
There total 9 articles about 9-(2,3,5-tri-O-benzoyl-β-L-ribofuranosyl)-N-palmitoylguanosine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
benzenesulfonamide; trimethylsilyl trifluoromethanesulfonate;
In
1,2-dichloro-ethane;
for 4h;
Heating;
DOI:10.1080/07328319808004239
- Guidance literature:
-
Multi-step reaction with 4 steps
1: HCl / 4 h
2: 90 percent / CH2Cl2; pyridine / 3 h
3: 9.5 g / sulphuric acid, acetic acid / 15 h / 0 - 5 °C
4: 2.) trimethylsilyl triflate / 1.) 1,2-dichloroethane, toluene, reflux, 30 min, 2.) 4 h
With
hydrogenchloride; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; acetic acid;
In
pyridine; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 27 percent / molybdenum(VI) oxide bis-2,4-pentanedionate / dimethylformamide / 24 h / 50 °C
2: HCl / 4 h
3: 90 percent / CH2Cl2; pyridine / 3 h
4: 9.5 g / sulphuric acid, acetic acid / 15 h / 0 - 5 °C
5: 2.) trimethylsilyl triflate / 1.) 1,2-dichloroethane, toluene, reflux, 30 min, 2.) 4 h
With
hydrogenchloride; MoO2(acetylacetonate)2; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; acetic acid;
In
pyridine; dichloromethane; N,N-dimethyl-formamide;
