Acetic acid (2R,3R,4R,5R)-4-acetoxy-5-acetoxymethyl-2-[6-oxo-1-(2,4,6-trimethyl-benzenesulfonyl)-1,6-dihydro-purin-9-yl]-tetrahydro-furan-3-yl ester

Base Information

Chemical Name:Acetic acid (2R,3R,4R,5R)-4-acetoxy-5-acetoxymethyl-2-[6-oxo-1-(2,4,6-trimethyl-benzenesulfonyl)-1,6-dihydro-purin-9-yl]-tetrahydro-furan-3-yl ester
CAS No.:863033-36-7
Molecular Formula:C₂₅H₂₈N₄O₁₀S
Molecular Weight:576.584
Hs Code.:

Acetic acid (2R,3R,4R,5R)-4-acetoxy-5-acetoxymethyl-2-[6-oxo-1-(2,4,6-trimethyl-benzenesulfonyl)-1,6-dihydro-purin-9-yl]-tetrahydro-furan-3-yl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid (2R,3R,4R,5R)-4-acetoxy-5-acetoxymethyl-2-[6-oxo-1-(2,4,6-trimethyl-benzenesulfonyl)-1,6-dihydro-purin-9-yl]-tetrahydro-furan-3-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Acetic acid (2R,3R,4R,5R)-4-acetoxy-5-acetoxymethyl-2-[6-oxo-1-(2,4,6-trimethyl-benzenesulfonyl)-1,6-dihydro-purin-9-yl]-tetrahydro-furan-3-yl ester

There total 1 articles about Acetic acid (2R,3R,4R,5R)-4-acetoxy-5-acetoxymethyl-2-[6-oxo-1-(2,4,6-trimethyl-benzenesulfonyl)-1,6-dihydro-purin-9-yl]-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 6979-94-8
2',3',5'-tri-O-acetyl-guanosine

: 863033-36-7
Acetic acid (2R,3R,4R,5R)-4-acetoxy-5-acetoxymethyl-2-[6-oxo-1-(2,4,6-trimethyl-benzenesulfonyl)-1,6-dihydro-purin-9-yl]-tetrahydro-furan-3-yl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetlet.2005.05.137

Reference yield:

: 863033-36-7
Acetic acid (2R,3R,4R,5R)-4-acetoxy-5-acetoxymethyl-2-[6-oxo-1-(2,4,6-trimethyl-benzenesulfonyl)-1,6-dihydro-purin-9-yl]-tetrahydro-furan-3-yl ester

: 121-44-8
triethylamine

: C₂₅H₃₁N₄⁽¹⁵⁾NO₁₀S*C₆H₁₅N

Guidance literature:: With potassium hydroxide; ammonium-¹⁵N hydrochloride; In water; acetonitrile; at 20 ℃;
DOI:10.1016/j.tetlet.2005.05.137

Reference yield:

: 863033-36-7
Acetic acid (2R,3R,4R,5R)-4-acetoxy-5-acetoxymethyl-2-[6-oxo-1-(2,4,6-trimethyl-benzenesulfonyl)-1,6-dihydro-purin-9-yl]-tetrahydro-furan-3-yl ester

: 4543-58-2
2,4,6-trimethylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / -30 - 20 °C

2: TFA / acetonitrile / 80 °C

With trifluoroacetic acid; In acetonitrile;
DOI:10.1016/j.tetlet.2005.05.137