C₃₅H₅₅NO₆Si

Base Information

Chemical Name:C₃₅H₅₅NO₆Si
CAS No.:1429226-42-5
Molecular Formula:C₃₅H₅₅NO₆Si
Molecular Weight:613.91
Hs Code.:

C<sub>35</sub>H<sub>55</sub>NO<sub>6</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₅H₅₅NO₆Si

Chemical Property:

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Technology Process of C₃₅H₅₅NO₆Si

There total 9 articles about C₃₅H₅₅NO₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1429226-41-4
C₃₅H₅₇NO₆Si

: 1429226-42-5
C₃₅H₅₅NO₆Si

Guidance literature:: With pyridine; Dess-Martin periodane; In dichloromethane; at 0 ℃; for 3.5h;
DOI:10.1016/j.tetlet.2013.01.110

Reference yield:

: C₂₈H₄₁NO₅

: 1429226-42-5
C₃₅H₅₅NO₆Si

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / water; 1,4-dioxane; methanol / 1 h / 0 - 20 °C

2: 1H-imidazole / dichloromethane / 1 h / 0 °C

3: sodium tetrahydroborate; calcium chloride / tetrahydrofuran / 3 h / 0 °C

4: Dess-Martin periodane; pyridine / dichloromethane / 3.5 h / 0 °C

With pyridine; 1H-imidazole; sodium tetrahydroborate; Dess-Martin periodane; triethylamine; calcium chloride; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water;
DOI:10.1016/j.tetlet.2013.01.110

Reference yield:

: 1429226-34-5
C₁₇H₂₇NO₄

: 1429226-42-5
C₃₅H₅₅NO₆Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C

2.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

3.1: copper(II) sulfate / dichloromethane / 18 h / 20 °C

4.1: lithium diisopropyl amide / hexane; tetrahydrofuran / 3 h / -78 °C

4.2: 60 h / -60 °C

5.1: hydrogenchloride / water; 1,4-dioxane; methanol / 1 h / 20 °C

6.1: triethylamine / water; 1,4-dioxane; methanol / 1 h / 0 - 20 °C

7.1: 1H-imidazole / dichloromethane / 1 h / 0 °C

8.1: sodium tetrahydroborate; calcium chloride / tetrahydrofuran / 3 h / 0 °C

9.1: Dess-Martin periodane; pyridine / dichloromethane / 3.5 h / 0 °C

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; hydrogenchloride; sodium tetrahydroborate; diisobutylaluminium hydride; Dess-Martin periodane; copper(II) sulfate; triethylamine; calcium chloride; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water;
DOI:10.1016/j.tetlet.2013.01.110