C₅₅H₇₇N₁₀O₁₃P

Base Information

• Chemical Name: C₅₅H₇₇N₁₀O₁₃P
• CAS No.: 946847-94-5
• Molecular Formula: C₅₅H₇₇N₁₀O₁₃P
• Molecular Weight: 1117.25
• Mol file: 946847-94-5.mol

Synonyms:

Chemical Property of C₅₅H₇₇N₁₀O₁₃P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₅H₇₇N₁₀O₁₃P

There total 14 articles about C₅₅H₇₇N₁₀O₁₃P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C21H40N2O9S → C55H77N10O13P (946847-94-5)

Guidance literature:

Multi-step reaction with 10 steps

1: NaN₃ / dimethylformamide / 90 °C

2: aq. LiOH / dioxane

3: EDCI; HOBt; i-Pr₂NEt / CH₂Cl₂

4: 80 percent / CuSO₄*5H₂O; sodium ascorbate / H₂O; 2-methyl-propan-2-ol

5: aq. LiOH / dioxane

6: EDCI; HOBt; i-Pr₂NEt / CH₂Cl₂

7: aq. HCl

8: EDCI; HOBt; i-Pr₂NEt / CH₂Cl₂

9: diethylamine / acetonitrile

10: EDCI; HOBt; i-Pr₂NEt / CH₂Cl₂

With hydrogenchloride; lithium hydroxide; sodium azide; benzotriazol-1-ol; copper(II) sulfate; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;

DOI:10.1016/j.bmcl.2007.04.096

Reference yield:

C24H40N6O7 (946847-87-6) → C55H77N10O13P (946847-94-5)

Guidance literature:

Multi-step reaction with 5 steps

1: EDCI; HOBt; i-Pr₂NEt / CH₂Cl₂

2: aq. HCl

3: EDCI; HOBt; i-Pr₂NEt / CH₂Cl₂

4: diethylamine / acetonitrile

5: EDCI; HOBt; i-Pr₂NEt / CH₂Cl₂

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile;

DOI:10.1016/j.bmcl.2007.04.096

Reference yield:

C19H35N5O6 (946847-81-0) → C55H77N10O13P (946847-94-5)

Guidance literature:

Multi-step reaction with 8 steps

1: EDCI; HOBt; i-Pr₂NEt / CH₂Cl₂

2: 80 percent / CuSO₄*5H₂O; sodium ascorbate / H₂O; 2-methyl-propan-2-ol

3: aq. LiOH / dioxane

4: EDCI; HOBt; i-Pr₂NEt / CH₂Cl₂

5: aq. HCl

6: EDCI; HOBt; i-Pr₂NEt / CH₂Cl₂

7: diethylamine / acetonitrile

8: EDCI; HOBt; i-Pr₂NEt / CH₂Cl₂

With hydrogenchloride; lithium hydroxide; benzotriazol-1-ol; copper(II) sulfate; sodium L-ascorbate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; water; acetonitrile; tert-butyl alcohol;

DOI:10.1016/j.bmcl.2007.04.096

upstream raw materials:

C₂₄H₄₀N₆O₇

C₃₃H₅₀N₈O₇

C₂₄H₃₄N₈O₅

C₄₅H₅₅N₉O₈