(3S,4S)-alanine Isoamylamide

Base Information

Chemical Name:(3S,4S)-alanine Isoamylamide
CAS No.:85613-70-3
Molecular Formula:C₂₅H₄₁N₃O₅
Molecular Weight:463.618
Hs Code.:

(3S,4S)-<N-(tert-Butyloxycarbonyl)-4-amino-3-hydroxyl-3-methyl-5-phenylpentanoyl>alanine Isoamylamide

Synonyms:

Suppliers and Price of (3S,4S)-alanine Isoamylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S)-alanine Isoamylamide

Chemical Property:

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Technology Process of (3S,4S)-alanine Isoamylamide

There total 8 articles about (3S,4S)-alanine Isoamylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.4%

: 85613-67-8
(S)-4-tert-Butoxycarbonylamino-3-hydroxy-3-methyl-5-phenyl-pentanoic acid

: 72155-60-3
(S)-2-amino-N-isopentylpropanamide hydrochloride

: 85613-70-3,85613-71-4
alanine Isoamylamide

: 85613-71-4
(3R,4S)-alanine Isoamylamide

: 85613-70-3
(3S,4S)-alanine Isoamylamide

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide; 2.) EtOAc, 3h, room temp.;
DOI:10.1021/jo00159a017

Reference yield: 63.4%

: 85613-67-8
(S)-4-tert-Butoxycarbonylamino-3-hydroxy-3-methyl-5-phenyl-pentanoic acid

: 72155-60-3
(S)-2-amino-N-isopentylpropanamide hydrochloride

: 85613-70-3,85613-71-4
alanine Isoamylamide

: 85613-71-4
(3R,4S)-alanine Isoamylamide

: 85613-70-3
(3S,4S)-alanine Isoamylamide

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide; 2.) EtOAc, 3h, room temp.;
DOI:10.1021/jo00159a017

Reference yield:

: 13139-15-6,53296-34-7
N-tert-butoxycarbonyl-L-leucine

: 85613-70-3
(3S,4S)-alanine Isoamylamide

Guidance literature:: Multi-step reaction with 4 steps

1: 43 percent / 1,2-dimethoxy-ethane; diethyl ether / 6 h / 0 - 5 °C

2: 77.6 percent / n-BuLi, iPr₂NH / hexane; tetrahydrofuran

3: 96.3 percent / 2 N NaOH

4: 63.4 percent / 1.) N-Methylmorpholine (NMM), 1-Hydroxybenzotriazole (HOBT), Dicyclohexylcarbodiimide (DCC) / 2.) EtOAc, 3h, room temp.

With 4-methyl-morpholine; sodium hydroxide; n-butyllithium; benzotriazol-1-ol; diisopropylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; hexane;
DOI:10.1021/jo00159a017