1,1-Dichloro-3-phenyl-2-propyne

Base Information

Chemical Name:1,1-Dichloro-3-phenyl-2-propyne
CAS No.:13524-09-9
Molecular Formula:C9H6Cl2
Molecular Weight:185.053
Hs Code.:
DSSTox Substance ID:DTXSID50569415
Nikkaji Number:J436.290J
Wikidata:Q82456564
Mol file:13524-09-9.mol

Synonyms:1,1-Dichloro-3-phenyl-2-propyne;13524-09-9;DTXSID50569415;(3,3-Dichloroprop-1-yn-1-yl)benzene

Suppliers and Price of 1,1-Dichloro-3-phenyl-2-propyne

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1,1-Dichloro-3-phenyl-2-propyne

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:183.9846556
Heavy Atom Count:11
Complexity:167

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C#CC(Cl)Cl

Technology Process of 1,1-Dichloro-3-phenyl-2-propyne

There total 5 articles about 1,1-Dichloro-3-phenyl-2-propyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2579-22-8
Phenylpropargyl aldehyde

: 13524-09-9
(3,3-dichloroprop-1-yn-1-yl)benzene

Guidance literature:: With phosphorus pentachloride;
DOI:10.1021/jo01349a517

Reference yield:

: 673-32-5
1-Phenylprop-1-yne

: 13524-09-9
(3,3-dichloroprop-1-yn-1-yl)benzene

Guidance literature:: 1-Phenylprop-1-yne; With n-butyllithium; In diethyl ether; N,N-dimethyl-formamide; at -40 - 20 ℃; for 0.5h; Inert atmosphere;

With phosphorus pentachloride; In dichloromethane; at -20 ℃; Inert atmosphere;
DOI:10.1021/ol302790e

Reference yield:

: 6142-95-6
phenylpropargyl aldehyde diethyl acetal

: 13524-09-9
(3,3-dichloroprop-1-yn-1-yl)benzene

Guidance literature:: With pyridine; formic acid; phosphorus pentachloride; Yield given. Multistep reaction; 1) CHCl₃, 40-45 deg C, 2) -20 deg C, 20-30 min;