4,5-dihydro-4-{4-(2-phenyl-1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-yl)butyl}-3-(3,4,5-trimethoxyphenyl)isoxazole

Base Information

• Chemical Name: 4,5-dihydro-4-{4-(2-phenyl-1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-yl)butyl}-3-(3,4,5-trimethoxyphenyl)isoxazole
• CAS No.: 154445-70-2
• Molecular Formula: C₂₄H₃₇B₁₀NO₄
• Molecular Weight: 511.672

Synonyms:

Chemical Property of 4,5-dihydro-4-{4-(2-phenyl-1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-yl)butyl}-3-(3,4,5-trimethoxyphenyl)isoxazole

Chemical Property:

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Safty Information:

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Technology Process of 4,5-dihydro-4-{4-(2-phenyl-1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-yl)butyl}-3-(3,4,5-trimethoxyphenyl)isoxazole

There total 1 articles about 4,5-dihydro-4-{4-(2-phenyl-1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-yl)butyl}-3-(3,4,5-trimethoxyphenyl)isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

2-hex-5-enyl-1-phenyl-1,2-dicarba-closo-dodecaborane(12) (154445-69-9) + 3,4,5-trimethoxybenzaldehyde oxime (39201-89-3) → 4,5-dihydro-4-{4-(2-phenyl-1,2-dicarba-closo-dodecaboran(12)-1-yl)butyl}-3-(3,4,5-trimethoxyphenyl)isoxazole (154445-70-2)

Guidance literature:

With NaOCl; H₂O; In dichloromethane; vigorous stirring of the oxime and the borane in CH2Cl2 together with aq. NaOCl for 16 h, addn. of further aq. NaOCl, 30 min; diluting with H2O, extn. 9CH2Cl2), evapn., chromy. of the residue (pentane-CH2Cl2 3:1, then CH2Cl2-ethyl acetate 10:1, then ethyl acetate), evapn. of the solvent from the second portion of eluate, isoxazole as an oily product;

DOI:10.1039/P19940000203

upstream raw materials:

2-hex-5-enyl-1-phenyl-1,2-dicarba-closo-dodecaborane⁽¹²⁾

3,4,5-trimethoxybenzaldehyde oxime

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