2,2,3,3-tetrachloro-1,1,1,4,4,4-hexakis(trimethylsilyl)tetragermane

Base Information

Chemical Name:2,2,3,3-tetrachloro-1,1,1,4,4,4-hexakis(trimethylsilyl)tetragermane
CAS No.:154319-54-7
Molecular Formula:C₁₈H₅₄Cl₄Ge₄Si₆
Molecular Weight:871.312
Hs Code.:

Synonyms:

Suppliers and Price of 2,2,3,3-tetrachloro-1,1,1,4,4,4-hexakis(trimethylsilyl)tetragermane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2,3,3-tetrachloro-1,1,1,4,4,4-hexakis(trimethylsilyl)tetragermane

Chemical Property:

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Technology Process of 2,2,3,3-tetrachloro-1,1,1,4,4,4-hexakis(trimethylsilyl)tetragermane

There total 1 articles about 2,2,3,3-tetrachloro-1,1,1,4,4,4-hexakis(trimethylsilyl)tetragermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Li⁽¹⁺⁾*Ge⁽²⁺⁾*3Si(CH₃)3^(1-)*2.5C₄H₈O=(C₄H₈O)2.5LiGe(Si(CH₃)3)3

: 10038-98-9
germaniumtetrachloride

: 104164-54-7
tris(trimethylsilyl)germane

: 104164-57-0
hexakis(trimethylsilyl)digermane

: 154319-54-7
2,2,3,3-tetrachloro-1,1,1,4,4,4-hexakis(trimethylsilyl)tetragermane

: 19372-30-6
tetrakis(trimethylsilyl)germanium

Guidance literature:: In hexane; Ar-atmosphere; dropwise addn. of GeCl4 to 2 equiv. of Li-compd. (-78°C, stirring (-78°C, 12 h), slow warming to ambient temp., stirring (36 h); product mixt. not sepd., detd. by (1)H-NMR spectroscopy;

Reference yield:

: 16853-85-3
lithium aluminium tetrahydride

: 154319-54-7
2,2,3,3-tetrachloro-1,1,1,4,4,4-hexakis(trimethylsilyl)tetragermane

: 104164-54-7
tris(trimethylsilyl)germane

: 104164-57-0
hexakis(trimethylsilyl)digermane

: 19372-30-6
tetrakis(trimethylsilyl)germanium

Guidance literature:: With HCl; In diethyl ether; Ar-atmosphere; room temp., 5 days; addn. of 10% HCl, extn. (ether); product mixt. not sepd., detd. by (1)H-NMR spectroscopy;