C₂₇H₃₂N₂O₅

Base Information

Chemical Name:C₂₇H₃₂N₂O₅
CAS No.:1333430-26-4
Molecular Formula:C₂₇H₃₂N₂O₅
Molecular Weight:464.561
Hs Code.:

C<sub>27</sub>H<sub>32</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₂₇H₃₂N₂O₅

Chemical Property:

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Technology Process of C₂₇H₃₂N₂O₅

There total 6 articles about C₂₇H₃₂N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 885524-92-5
3-formyl-2-methylindole-1-carboxylic acid tert-butyl ester

: 1333430-26-4
C₂₇H₃₂N₂O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C

1.2: 4 h / 0 °C

2.1: diisobutylaluminium hydride / n-heptane; toluene / 3.33 h / -78 °C

3.1: (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; benzoic acid / toluene / 40 h / 70 °C

4.1: sodium tetrahydroborate

With sodium tetrahydroborate; n-butyllithium; (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; diisobutylaluminium hydride; benzoic acid; In tetrahydrofuran; hexane; n-heptane; toluene; 1.1: Wittig reaction / 1.2: Wittig reaction / 3.1: Diels-Alder reaction;
DOI:10.1021/ja206517s

Reference yield:

: 5416-80-8
2-methyl-1H-indole-3-carbaldehyde

: 1333430-26-4
C₂₇H₃₂N₂O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: dmap / acetonitrile / 0 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C

2.2: 4 h / 0 °C

3.1: diisobutylaluminium hydride / n-heptane; toluene / 3.33 h / -78 °C

4.1: (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; benzoic acid / toluene / 40 h / 70 °C

5.1: sodium tetrahydroborate

With dmap; sodium tetrahydroborate; n-butyllithium; (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; diisobutylaluminium hydride; benzoic acid; In tetrahydrofuran; hexane; n-heptane; toluene; acetonitrile; 2.1: Wittig reaction / 2.2: Wittig reaction / 4.1: Diels-Alder reaction;
DOI:10.1021/ja206517s

Reference yield:

: 1333429-62-1
(E)-tert-butyl 2-methyl-3-(3-oxoprop-1-en-1-yl)-1H-indole-1-carboxylate

: 1333430-26-4
C₂₇H₃₂N₂O₅

Guidance literature:: Multi-step reaction with 2 steps

1: (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; benzoic acid / toluene / 40 h / 70 °C

2: sodium tetrahydroborate

With sodium tetrahydroborate; (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; benzoic acid; In toluene; 1: Diels-Alder reaction;
DOI:10.1021/ja206517s