5-amino-4-methyl-2-phenylfuro[2,3-d]pyrimidine-6-carboazide

Base Information

Chemical Name:5-amino-4-methyl-2-phenylfuro[2,3-d]pyrimidine-6-carboazide
CAS No.:869370-44-5
Molecular Formula:C₁₄H₁₀N₆O₂
Molecular Weight:294.272
Hs Code.:

Synonyms:

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Chemical Property of 5-amino-4-methyl-2-phenylfuro[2,3-d]pyrimidine-6-carboazide

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Technology Process of 5-amino-4-methyl-2-phenylfuro[2,3-d]pyrimidine-6-carboazide

There total 5 articles about 5-amino-4-methyl-2-phenylfuro[2,3-d]pyrimidine-6-carboazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2228-12-8
4-methyl-6-mercapto-2-phenylpyrimidine-5-carbonitrile

: 869370-44-5
5-amino-4-methyl-2-phenylfuro[2,3-d]pyrimidine-6-carboazide

Guidance literature:: Multi-step reaction with 5 steps

1.1: 85 percent / K₂CO₃ / ethanol / 3 h / Heating

2.1: aq. NaOH / ethanol / 4 h / Heating

2.2: acetone / 4 h / Heating

3.1: 83 percent / NaOEt / ethanol / 1 h / Heating

4.1: 73 percent / hydrazine hydrate / ethanol / 3 h / Heating

5.1: aq. NaNO₂; glacial acetic acid / 2 h

With sodium hydroxide; sodium ethanolate; potassium carbonate; hydrazine hydrate; acetic acid; sodium nitrite; In ethanol;
DOI:10.1002/jccs.200400198

Reference yield:

: 333722-72-8
6-ethylthio-4-methyl-2-phenylpyrimidine-5-carbonitrile

: 869370-44-5
5-amino-4-methyl-2-phenylfuro[2,3-d]pyrimidine-6-carboazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: aq. NaOH / ethanol / 4 h / Heating

1.2: acetone / 4 h / Heating

2.1: 83 percent / NaOEt / ethanol / 1 h / Heating

3.1: 73 percent / hydrazine hydrate / ethanol / 3 h / Heating

4.1: aq. NaNO₂; glacial acetic acid / 2 h

With sodium hydroxide; sodium ethanolate; hydrazine hydrate; acetic acid; sodium nitrite; In ethanol;
DOI:10.1002/jccs.200400198

Reference yield:

: 717840-92-1
5-amino-4-methyl-2-phenylfuro[2,3-d]pyrimidine-6-carboxylate

: 869370-44-5
5-amino-4-methyl-2-phenylfuro[2,3-d]pyrimidine-6-carboazide

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / hydrazine hydrate / ethanol / 3 h / Heating

2: aq. NaNO₂; glacial acetic acid / 2 h

With hydrazine hydrate; acetic acid; sodium nitrite; In ethanol;
DOI:10.1002/jccs.200400198