bis(2,6-di-t-butyl-4-methoxyphenoxo)trimethyltantalum(V)

Base Information

Chemical Name:bis(2,6-di-t-butyl-4-methoxyphenoxo)trimethyltantalum(V)
CAS No.:100447-72-1
Molecular Formula:C₃₃H₅₅O₄Ta
Molecular Weight:696.745
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(2,6-di-t-butyl-4-methoxyphenoxo)trimethyltantalum(V)

Chemical Property:

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Technology Process of bis(2,6-di-t-butyl-4-methoxyphenoxo)trimethyltantalum(V)

There total 1 articles about bis(2,6-di-t-butyl-4-methoxyphenoxo)trimethyltantalum(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100447-73-2
Ta{4-methoxy-2,6-di-tert-bu-tert-butylphenoxide}2Cl₃

: 917-54-4
methyllithium

: 100447-72-1
bis(2,6-di-t-butyl-4-methoxyphenoxo)trimethyltantalum(V)

Guidance literature:: In benzene; byproducts: LiCl; to a soln of Ta compd. is added LiCH3, the suspn. is stirred at 25°C for 30 min (N2 atm.); filtered, evapd. in vac.; elem. anal.;
DOI:10.1021/ja00267a020

Reference yield:

: 100447-72-1
bis(2,6-di-t-butyl-4-methoxyphenoxo)trimethyltantalum(V)

: 100447-75-4
Ta(OC₁₄H₂₀OCH₃)2(CH₃)(CH₂)

Guidance literature:: In not given; Irradiation (UV/VIS); photolysis of soln. of complex in benzene or hexane at 10°C for 1 h (N2 atm.); not sepd., detected by NMR spectra;
DOI:10.1021/ja00267a020

Reference yield:

: 100447-72-1
bis(2,6-di-t-butyl-4-methoxyphenoxo)trimethyltantalum(V)

: 100447-74-3
Ta(OC₆H₂(OCH₃)(C₄H₉)C(CH₃)2CH₂)(OC₁₄H₂₀OCH₃)(CH₃)2

Guidance literature:: In toluene; byproducts: CH4; toluene soln. of complex was heated in a closed flask for 24 h at 95°C (N2 atm.); evapd. in vac.;
DOI:10.1021/ja00267a020