Bmv-Phe(I)-D-Lys(Boc)-Phe-OtBu

Base Information

Chemical Name:Bmv-Phe(I)-D-Lys(Boc)-Phe-OtBu
CAS No.:87325-39-1
Molecular Formula:C₄₃H₅₅IN₄O₇
Molecular Weight:866.837
Hs Code.:

Synonyms:

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Chemical Property of Bmv-Phe(I)-D-Lys(Boc)-Phe-OtBu

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Technology Process of Bmv-Phe(I)-D-Lys(Boc)-Phe-OtBu

There total 1 articles about Bmv-Phe(I)-D-Lys(Boc)-Phe-OtBu which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: H-D-Lys(Boc)-Phe-OtBu

: Bmv-Phe(I)-OH

: 87325-39-1
Bmv-Phe(I)-D-Lys(Boc)-Phe-OtBu

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; 1.) 0 deg C, 2 h; 2.) r.t., overnight;
DOI:10.1002/recl.19831020505

Reference yield:

: 87325-39-1
Bmv-Phe(I)-D-Lys(Boc)-Phe-OtBu

: 774493-73-1
Phe(I)-D-Lys(Boc)-Phe-OtBu

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; for 0.5h; Ambient temperature;
DOI:10.1002/recl.19831020505

Reference yield:

: 87325-39-1
Bmv-Phe(I)-D-Lys(Boc)-Phe-OtBu

: 87325-34-6
H-Met(O₂)-Glu-His-Phe(I)-D-Lys-Phe-OH

Guidance literature:: Multi-step reaction with 3 steps

1: 6 N HCl / tetrahydrofuran; H₂O / 0.5 h / Ambient temperature

2: 1.) 4.4 N HCl, THF, isopentyl nitrite; 2.) N-ethylmorpholine / 1.) DMF, -20 deg C, 20 min; 2.) 5 deg C, 3 d

3: 728 mg / TFA, water / 0.5 h / Ambient temperature

With tetrahydrofuran; N-ethylmorpholine;; hydrogenchloride; water; trifluoroacetic acid; isopentyl nitrite; In tetrahydrofuran; water;
DOI:10.1002/recl.19831020505