dichlorothionitrobis(triphenyl phosphito)cobalt(III)

Base Information

Chemical Name:dichlorothionitrobis(triphenyl phosphito)cobalt(III)
CAS No.:80028-18-8
Molecular Formula:C₃₆H₃₀Cl₂CoNO₇P₂S
Molecular Weight:812.549
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dichlorothionitrobis(triphenyl phosphito)cobalt(III)

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Technology Process of dichlorothionitrobis(triphenyl phosphito)cobalt(III)

There total 1 articles about dichlorothionitrobis(triphenyl phosphito)cobalt(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 105454-00-0,105453-99-4,5964-00-1
trithiazyl trichloride

: 24651-64-7,99883-28-0,41089-90-1
hydridotetrakis(triphenylphosphite)cobalt(I)

: 80028-18-8
dichlorothionitrobis(triphenyl phosphito)cobalt(III)

Guidance literature:: In tetrahydrofuran; byproducts: S4N4; (NSCl)3 in THF was slowly added with stirring to the THF soln. of Co complex at 30°C under dry Ar, stirring was continued for ca. 30 min; green soln. was concd. at room temp. under reduced pressure, filtered under Ar, then degassed petroleum ether was added, the ppt. was washed with water and dried in air; elem. anal., soln. after washing was concd., cooled, S4N4 needles sepd. out;