Cu⁽¹⁺⁾*Cl^(1-)*(CH₃C₅H₃N)3CH=CuCl((CH₃C₅H₃N)3CH)

Base Information

• Chemical Name: Cu⁽¹⁺⁾*Cl^(1-)*(CH₃C₅H₃N)3CH=CuCl((CH₃C₅H₃N)3CH)
• CAS No.: 258329-03-2
• Molecular Formula: C₁₉H₁₉N₃*Cl*Cu
• Molecular Weight: 388.379
• Mol file: 258329-03-2.mol

Synonyms:

Chemical Property of Cu⁽¹⁺⁾*Cl^(1-)*(CH₃C₅H₃N)3CH=CuCl((CH₃C₅H₃N)3CH)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Cu⁽¹⁺⁾*Cl^(1-)*(CH₃C₅H₃N)3CH=CuCl((CH₃C₅H₃N)3CH)

There total 1 articles about Cu⁽¹⁺⁾*Cl^(1-)*(CH₃C₅H₃N)3CH=CuCl((CH₃C₅H₃N)3CH) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

ammonium hexafluorophosphate + tris(6-methyl-2-pyridyl)methane (201339-89-1) + copper dichloride → Cu3Cl((CH3C5H3N)3CO)3(2+)*2PF6(1-)*CH3CN*CH2Cl2*C6H6=Cu3Cl((CH3C5H3N)3CO)3(PF6)2*C6H6*CH3CN*CH2Cl2 + Cu(1+)*Cl(1-)*(CH3C5H3N)3CH=CuCl((CH3C5H3N)3CH) (258329-03-2)

Guidance literature:

With NaOH; In methanol; to soln. of CuCl2 in MeOH was added soln. of ligand in MeOH with stirring for 24 h under air, soln. of NaOH in MeOH was added, mixt. was stirred at room temp. for 18 h, filtered, NH4PF6 was added; filtered, recrystd. from MeCN/CH2Cl2/C6H6; elem. anal.;

DOI:10.1021/ic990331g

upstream raw materials:

tris(6-methyl-2-pyridyl)methane

Refernces