pentachlorophenyl-2,4-pentanedionate trimethylphosphine nickel(II)

Base Information

Chemical Name:pentachlorophenyl-2,4-pentanedionate trimethylphosphine nickel(II)
CAS No.:114171-79-8
Molecular Formula:C₁₄H₁₆Cl₅NiO₂P
Molecular Weight:483.209
Hs Code.:

Synonyms:

Suppliers and Price of pentachlorophenyl-2,4-pentanedionate trimethylphosphine nickel(II)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of pentachlorophenyl-2,4-pentanedionate trimethylphosphine nickel(II)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of pentachlorophenyl-2,4-pentanedionate trimethylphosphine nickel(II)

There total 1 articles about pentachlorophenyl-2,4-pentanedionate trimethylphosphine nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 82647-54-9
[NiCl(C₆Cl₅)(P(CH₃)3)2]

: thallium(I) 2,4-pentanedionate

: 114171-79-8
pentachlorophenyl-2,4-pentanedionate trimethylphosphine nickel(II)

Guidance literature:: In dichloromethane; byproducts: TlCl, P(CH3)3; under N2; a soln. of trans-(NiCl(C6Cl5)(PMe3)2) in CH2Cl2 is added to asuspension of Tl(acac) in CH2Cl2, mixt. is stirred at room temp. for a few min; TlCl so formed is filtered, evapd. in vac. and the residue is treated with EtOH, ppt. is recrystd. from CH2Cl2/EtOH; elem. anal.;
DOI:10.1016/S0020-1693(00)90443-2