Technology Process of Pentanoic acid, 5-(3-butoxyphenoxy)-, methyl ester
There total 1 articles about Pentanoic acid, 5-(3-butoxyphenoxy)-, methyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate; sodium iodide;
In
acetone;
for 3h;
Heating;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) diisobutylaluminium hydride, 2.) 5percent methanolic HCl / 1.) toluene, -78 deg, 4 h, 2.) 5percent methanolic HCl
2: 77 percent / hydroxylamine hydrochloride / ethanol; pyridine / 3 h / 40 °C
With
hydrogenchloride; hydroxylamine hydrochloride; diisobutylaluminium hydride;
In
pyridine; ethanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) diisobutylaluminium hydride, 2.) 5percent methanolic HCl / 1.) toluene, -78 deg, 4 h, 2.) 5percent methanolic HCl
2: 77 percent / hydroxylamine hydrochloride / ethanol; pyridine / 3 h / 40 °C
3: 1.) borane-pyridine complex, 2.) dimethylaminopyridine, / 1.) ethanol, 0 deg, 10 min., 2.) pyridine, 20 deg, 3 h
4: 98 percent / triethylamine / methanol / 4 h / Ambient temperature
With
hydrogenchloride; dmap; borane pyridine; hydroxylamine hydrochloride; diisobutylaluminium hydride; triethylamine;
In
pyridine; methanol; ethanol;
