5-(4-(rhenium(I)tricarbonyl(3-picoline)-4-methyl-2,2'-bipyridine-4'-carboxyamidyl)phenyl)-10,15,20-triphenylporphyrinatozinc(II) trifluoromethanesulfonate

Base Information

Chemical Name:5-(4-(rhenium(I)tricarbonyl(3-picoline)-4-methyl-2,2'-bipyridine-4'-carboxyamidyl)phenyl)-10,15,20-triphenylporphyrinatozinc(II) trifluoromethanesulfonate
CAS No.:444166-81-8
Molecular Formula:CF₃O₃S*C₆₅H₄₄N₈O₄ReZn
Molecular Weight:1401.78
Hs Code.:

5-(4-(rhenium(I)tricarbonyl(3-picoline)-4-methyl-2,2'-bipyridine-4'-carboxyamidyl)phenyl)-10,15,20-triphenylporphyrinatozinc(II) trifluoromethanesulfonate

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Chemical Property of 5-(4-(rhenium(I)tricarbonyl(3-picoline)-4-methyl-2,2'-bipyridine-4'-carboxyamidyl)phenyl)-10,15,20-triphenylporphyrinatozinc(II) trifluoromethanesulfonate

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Technology Process of 5-(4-(rhenium(I)tricarbonyl(3-picoline)-4-methyl-2,2'-bipyridine-4'-carboxyamidyl)phenyl)-10,15,20-triphenylporphyrinatozinc(II) trifluoromethanesulfonate

There total 1 articles about 5-(4-(rhenium(I)tricarbonyl(3-picoline)-4-methyl-2,2'-bipyridine-4'-carboxyamidyl)phenyl)-10,15,20-triphenylporphyrinatozinc(II) trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 444159-73-3
5-(4-(rhenium⁽⁰⁾tricarbonyl(3-picoline)-4-methyl-2,2'-bipyridine-4'-carboxyamidyl)phenyl)-10,15,20-triphenylporphyrinatozinc

: 444166-81-8
5-(4-(rhenium(I)tricarbonyl(3-picoline)-4-methyl-2,2'-bipyridine-4'-carboxyamidyl)phenyl)-10,15,20-triphenylporphyrinatozinc(II) trifluoromethanesulfonate

Guidance literature:: With air; In tetrahydrofuran; exposure THF soln. of zinc compd. to air; IR monitoring;
DOI:10.1039/b806267f

Reference yield:

: 444166-81-8
5-(4-(rhenium(I)tricarbonyl(3-picoline)-4-methyl-2,2'-bipyridine-4'-carboxyamidyl)phenyl)-10,15,20-triphenylporphyrinatozinc(II) trifluoromethanesulfonate

: 444159-73-3
5-(4-(rhenium⁽⁰⁾tricarbonyl(3-picoline)-4-methyl-2,2'-bipyridine-4'-carboxyamidyl)phenyl)-10,15,20-triphenylporphyrinatozinc

Guidance literature:: With triethylamine; In tetrahydrofuran; Irradiation (UV/VIS); photolysis at >495 or >400 nm of THF soln. of porphyrin deriv. containing 5% triethylamine and 100 equiv. of picoline; IR monitoring and ESR;
DOI:10.1039/b806267f

Reference yield:

: 444166-81-8
5-(4-(rhenium(I)tricarbonyl(3-picoline)-4-methyl-2,2'-bipyridine-4'-carboxyamidyl)phenyl)-10,15,20-triphenylporphyrinatozinc(II) trifluoromethanesulfonate

: 1112-67-0
tetrabutyl-ammonium chloride

: 1065473-89-3
5-(4-(rhenium(I)tricarbonylchloride-4-methyl-2,2'-bipyridine-4'-carboxyamidyl)phenyl)-10,15,20-triphenylporphyrinatozinc

Guidance literature:: With triethylamine; In tetrahydrofuran; Irradiation (UV/VIS); photolysis at >495 nm of THF soln. of porphyrin deriv. containing 20 equiv. of triethylamine and chloride salt; IR monitoring;
DOI:10.1039/b806267f