Triethylammonium-6-benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)phosphat>

Base Information

• Chemical Name: Triethylammonium-6-benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)phosphat>
• CAS No.: 80727-22-6
• Molecular Formula: C₆H₁₅N*C₇₈H₈₄Cl₂N₁₀O₁₆P₂Si₂
• Molecular Weight: 1707.8

Synonyms:

Chemical Property of Triethylammonium-6-benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)phosphat>

Chemical Property:

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Useful:

Technology Process of Triethylammonium-6-benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)phosphat>

There total 1 articles about Triethylammonium-6-benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)phosphat> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

N6-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'->-N6-benzoyl-2'-O-(tert-butyldimetylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyanethyl)phosphat (75085-67-5) + triethylamine (121-44-8) → Triethylammonium-6-benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N6-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)phosphat> (80727-22-6)

Guidance literature:

In pyridine; for 2.5h; Ambient temperature;

Reference yield:

N6,N6,2'-O,3'-O-tetrabenzoyladenosine (58463-04-0) + Triethylammonium-6-benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N6-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)phosphat> (80727-22-6) → N6-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N6-benzoyl-2'-O-(tert-butyldimethylsilyl)adenylyl<3'-P-(2-chlorphenyl)>-5'>-N6,N6,2'-O,3'-O-tetrabenzoyladenosin (75085-69-7)

Guidance literature:

With 1-(2,4,6-triisopropylbenzenesulfonyl)-3-nitro-1,2,4-triazole; Yield given. Multistep reaction; 1) pyridine, heating; 2) pyridine, 12 h at room temp.;

upstream raw materials:

N⁶-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'->-N⁶-benzoyl-2'-O-(tert-butyldimetylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyanethyl)phosphat

triethylamine

Downstream raw materials:

N⁶-Benzoyl-3'-O-tert-butyldimethylsilyl-5'-O-(4-methoxytrityl)adenylyl<2'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2'-O-(tert-butyldimethylsilyl)adenylyl<3'-P-(2-chlorphenyl)>-5'>-N⁶,N⁶,2'-O,3'-O-tetrabenzoyladenosin

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