Technology Process of Acetaldehyde, (3-phenoxyphenoxy)-, oxime, (Z)-
There total 3 articles about Acetaldehyde, (3-phenoxyphenoxy)-, oxime, (Z)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride;
In
pyridine; ethanol;
at 40 ℃;
for 3h;
Title compound not separated from byproducts;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 91 percent / K2CO3, NaI / acetone / 10 h / Heating
2: 1.) diisobutylaluminium hydride, 2.) 5percent methanolic HCl / 1.) toluene, -78 deg, 4 h, 2.) 5percent methanolic HCl
3: hydroxylamine hydrochloride / ethanol; pyridine / 3 h / 40 °C
With
hydrogenchloride; hydroxylamine hydrochloride; diisobutylaluminium hydride; potassium carbonate; sodium iodide;
In
pyridine; ethanol; acetone;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) diisobutylaluminium hydride, 2.) 5percent methanolic HCl / 1.) toluene, -78 deg, 4 h, 2.) 5percent methanolic HCl
2: hydroxylamine hydrochloride / ethanol; pyridine / 3 h / 40 °C
With
hydrogenchloride; hydroxylamine hydrochloride; diisobutylaluminium hydride;
In
pyridine; ethanol;
