Technology Process of Acetamide, N-(acetyloxy)-N-[2-(3-methoxyphenoxy)ethyl]-
There total 4 articles about Acetamide, N-(acetyloxy)-N-[2-(3-methoxyphenoxy)ethyl]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 86 percent / K2CO3, NaI / acetone / 6 h / Heating
2: 1.) diisobutylaluminium hydride, 2.) 5percent methanolic HCl / 1.) toluene, -78 deg, 4 h, 2.) 5percent methanolic HCl
3: 56 percent / hydroxylamine hydrochloride / ethanol; pyridine / 3 h / 40 °C
4: 1.) borane-pyridine complex, 2.) dimethylaminopyridine / 1.) ethanol, 0 deg, 10 min., 2.) pyridine, 20 deg, 3 h
With
hydrogenchloride; dmap; borane pyridine; hydroxylamine hydrochloride; diisobutylaluminium hydride; potassium carbonate; sodium iodide;
In
pyridine; ethanol; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) diisobutylaluminium hydride, 2.) 5percent methanolic HCl / 1.) toluene, -78 deg, 4 h, 2.) 5percent methanolic HCl
2: 56 percent / hydroxylamine hydrochloride / ethanol; pyridine / 3 h / 40 °C
3: 1.) borane-pyridine complex, 2.) dimethylaminopyridine / 1.) ethanol, 0 deg, 10 min., 2.) pyridine, 20 deg, 3 h
With
hydrogenchloride; dmap; borane pyridine; hydroxylamine hydrochloride; diisobutylaluminium hydride;
In
pyridine; ethanol;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 56 percent / hydroxylamine hydrochloride / ethanol; pyridine / 3 h / 40 °C
2: 1.) borane-pyridine complex, 2.) dimethylaminopyridine / 1.) ethanol, 0 deg, 10 min., 2.) pyridine, 20 deg, 3 h
With
dmap; borane pyridine; hydroxylamine hydrochloride;
In
pyridine; ethanol;
