[5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(4-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾;O⁽¹⁾O⁽³⁾O⁽¹²⁾O⁽¹⁴⁾]nickel(II)zinc(II)hydrate

Base Information

• Chemical Name: [5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(4-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾;O⁽¹⁾O⁽³⁾O⁽¹²⁾O⁽¹⁴⁾]nickel(II)zinc(II)hydrate
• CAS No.: 60117-00-2
• Molecular Formula: C₂₆H₂₄N₂NiO₄Zn*H₂O
• Molecular Weight: 570.583
• Mol file: 60117-00-2.mol

Synonyms:

Chemical Property of [5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(4-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾;O⁽¹⁾O⁽³⁾O⁽¹²⁾O⁽¹⁴⁾]nickel(II)zinc(II)hydrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(4-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾;O⁽¹⁾O⁽³⁾O⁽¹²⁾O⁽¹⁴⁾]nickel(II)zinc(II)hydrate

There total 1 articles about [5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(4-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾;O⁽¹⁾O⁽³⁾O⁽¹²⁾O⁽¹⁴⁾]nickel(II)zinc(II)hydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

[5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato(2-)-N(6)N(9)O(3)O(12)]nickel(II) (55998-67-9) + zinc(II) acetate dihydrate (5970-45-6) → [5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato(4-)-N(6)N(9)O(3)O(12);O(1)O(3)O(12)O(14)]nickel(II)zinc(II)hydrate (60117-00-2)

Guidance literature:

In ethanol; acetone; addn. of monometallic complex (in hot Me2CO) to metal acetate (in EtOH),warming on steam-bath for 5 min; pptn. on cooling, collection (filtration), drying (vac., over silica gel); elem. anal.;

DOI:10.1039/DT9770002109

upstream raw materials:

[5,10-dimethyl-1,14-diphenyl-6,9-diazatetradeca-4,10-diene-1,3,12,14-tetraonato^(2-)-N⁽⁶⁾N⁽⁹⁾O⁽³⁾O⁽¹²⁾]nickel(II)

zinc(II) acetate dihydrate