[bis(dicobalt hexacarbonyl)-(μ-η2-C6H10OHCC)2]

Base Information

Chemical Name:[bis(dicobalt hexacarbonyl)-(μ-η2-C6H10OHCC)2]
CAS No.:508193-61-1
Molecular Formula:C₂₈H₂₂Co₄O₁₄
Molecular Weight:818.447
Hs Code.:

Synonyms:

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Chemical Property of [bis(dicobalt hexacarbonyl)-(μ-η2-C6H10OHCC)2]

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Technology Process of [bis(dicobalt hexacarbonyl)-(μ-η2-C6H10OHCC)2]

There total 2 articles about [bis(dicobalt hexacarbonyl)-(μ-η2-C6H10OHCC)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5768-10-5
1,4-bis(1-hydroxycyclohexyl)buta-1,3-diyne

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 508193-61-1
[bis(dicobalt hexacarbonyl)-(μ-η2-C6H10OHCC)2]

Guidance literature:: In diethyl ether; byproducts: CO; to a stirred soln. of the diyne in diethyl ether added two equiv. of Co2(CO)8 in small portions under a flow of argon, stirring for 6 h; silica-gel column chromy. (4:1 hexane:ethyl acetate);
DOI:10.1039/b206295j

Reference yield:

: 5768-10-5
1,4-bis(1-hydroxycyclohexyl)buta-1,3-diyne

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 508193-63-3
[(dicobalt hexacarbonyl)-(μ-η2-C6H10OHCCCCC6H10OH)]

: 508193-61-1
[bis(dicobalt hexacarbonyl)-(μ-η2-C6H10OHCC)2]

Guidance literature:: In diethyl ether; byproducts: CO; to a stirred soln. of the diyne in diethyl ether added one equiv. of Co2(CO)8 in small portions under a flow of argon, stirring for 6 h; silica-gel column chromy. (4:1 hexane:ethyl acetate);
DOI:10.1039/b206295j

Reference yield:

: 508193-61-1
[bis(dicobalt hexacarbonyl)-(μ-η2-C6H10OHCC)2]

: 508193-64-4
[bis(dicobalt hexacarbonyl)-(μ-η2-C6H9CC)2]

Guidance literature:: tetrafluoroboric acid; In dichloromethane; byproducts: H2O; to a soln. of the complex in dichloromethane at -78 °C under argon added five drops of 48% HBF4 in ether, warming to room temp., stirringfor 2 h; silica-gel column chromy. (hexane);
DOI:10.1039/b206295j