(diphenylphosphinoethyl)cyclopentadienyllutetium anthracenide tetrahydrofuranate

Base Information

Chemical Name:(diphenylphosphinoethyl)cyclopentadienyllutetium anthracenide tetrahydrofuranate
CAS No.:1130415-39-2
Molecular Formula:C₃₇H₃₆LuOP
Molecular Weight:702.633
Hs Code.:

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Chemical Property of (diphenylphosphinoethyl)cyclopentadienyllutetium anthracenide tetrahydrofuranate

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Technology Process of (diphenylphosphinoethyl)cyclopentadienyllutetium anthracenide tetrahydrofuranate

There total 1 articles about (diphenylphosphinoethyl)cyclopentadienyllutetium anthracenide tetrahydrofuranate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.8%

: lutetium trichloride-tetrahydrofuran(1/3)

: 1001666-33-6
sodium diphenylphosphinoethylcyclopentadienide

: 11065-56-8
disodium 9,10-dihydroanthracenediide

: 1130415-39-2
(diphenylphosphinoethyl)cyclopentadienyllutetium anthracenide tetrahydrofuranate

Guidance literature:: In tetrahydrofuran; (vac.); addn. of THF soln. of sodium cyclopentadienide deriv. to suspn. of lutetium chloride in anhyd. THF, stirring for 10 min, addn. of THF soln. of anthracenide deriv., stirring for 6 h; separating soln. from ppt., evapn., washing with petroleum ether, recrystn. (THF), elem. anal.;
DOI:10.1007/s11172-007-0271-1