C₂₄H₃₁N₅O₄

Base Information

Chemical Name:C₂₄H₃₁N₅O₄
CAS No.:1344675-01-9
Molecular Formula:C₂₄H₃₁N₅O₄
Molecular Weight:453.541
Hs Code.:

C<sub>24</sub>H<sub>31</sub>N<sub>5</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₃₁N₅O₄

Chemical Property:

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Technology Process of C₂₄H₃₁N₅O₄

There total 9 articles about C₂₄H₃₁N₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1344675-49-5
C₁₃H₁₉ClN₂O₃

: 1344675-01-9
C₂₄H₃₁N₅O₄

Guidance literature:: Multi-step reaction with 7 steps

1: water; lithium hydroxide / 1,2-dimethoxyethane / 23 °C

2: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 23 °C

3: ammonium hydroxide / water / 23 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,4-dioxane; water / Reflux

5: sodium hydride / N,N-dimethyl-formamide / 0 - 75 °C

6: trichlorophosphate / 100 °C

7: dichloromethane / 23 °C

With ammonium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; water; sodium hydride; sodium carbonate; N,N-dimethyl-formamide; lithium hydroxide; trichlorophosphate; In 1,4-dioxane; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; 4: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.08.106

Reference yield:

: 1344675-50-8
C₁₁H₁₅ClN₂O₃

: 1344675-01-9
C₂₄H₃₁N₅O₄

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 23 °C

2: ammonium hydroxide / water / 23 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,4-dioxane; water / Reflux

4: sodium hydride / N,N-dimethyl-formamide / 0 - 75 °C

5: trichlorophosphate / 100 °C

6: dichloromethane / 23 °C

With ammonium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; sodium hydride; sodium carbonate; N,N-dimethyl-formamide; trichlorophosphate; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; 3: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.08.106

Reference yield:

: 1344675-51-9
C₁₁H₁₆ClN₃O₂

: 1344675-01-9
C₂₄H₃₁N₅O₄

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,4-dioxane; water / Reflux

2: sodium hydride / N,N-dimethyl-formamide / 0 - 75 °C

3: trichlorophosphate / 100 °C

4: dichloromethane / 23 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; sodium carbonate; trichlorophosphate; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; 1: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.08.106