Technology Process of 2-(3-methyl)secbutyl-6-isopropylphenol
There total 6 articles about 2-(3-methyl)secbutyl-6-isopropylphenol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium 10% on activated carbon;
In
tetrahydrofuran;
at 20 ℃;
under 2942.29 - 3677.86 Torr;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dmap / dichloromethane / 2 h / 20 °C
2.1: aluminum (III) chloride / carbon disulfide / 20 - 70 °C
3.1: magnesium / iodine / diethyl ether / 20 °C / Inert atmosphere
3.2: 0 °C / Inert atmosphere; Reflux
3.3: 0 °C
4.1: toluene-4-sulfonic acid / dichloromethane / 24 h / 20 °C
5.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 20 °C / 2942.29 - 3677.86 Torr
With
dmap; aluminum (III) chloride; hydrogen; toluene-4-sulfonic acid; magnesium;
palladium 10% on activated carbon; iodine;
In
tetrahydrofuran; carbon disulfide; diethyl ether; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: water; lithium hydroxide / tetrahydrofuran / 20 °C
2.1: dmap / dichloromethane / 2 h / 20 °C
3.1: aluminum (III) chloride / carbon disulfide / 20 - 70 °C
4.1: magnesium / iodine / diethyl ether / 20 °C / Inert atmosphere
4.2: 0 °C / Inert atmosphere; Reflux
4.3: 0 °C
5.1: toluene-4-sulfonic acid / dichloromethane / 24 h / 20 °C
6.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 20 °C / 2942.29 - 3677.86 Torr
With
dmap; aluminum (III) chloride; water; hydrogen; toluene-4-sulfonic acid; magnesium; lithium hydroxide;
palladium 10% on activated carbon; iodine;
In
tetrahydrofuran; carbon disulfide; diethyl ether; dichloromethane;