Technology Process of (3S,4S,6Z,9Z)-3-benzoyloxy-4-tosyloxynonadeca-6,9-diene
There total 11 articles about (3S,4S,6Z,9Z)-3-benzoyloxy-4-tosyloxynonadeca-6,9-diene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) ethylmagnesium bromide, 2.) CuCl
2: 88 percent / aq. silver nitrate / ethanol / 1 h
3: 1.) BuLi, 2.) borontrifluoride etherate / 1.) THF, hexane, -60 deg C, 15 min, 2.) THF, -70 deg C, 30 min
4: 62 percent / H2 / Lindlar catalyst / methanol / 1 h
5: 73 percent / pyridine / 24 h / 0 °C
With
pyridine; n-butyllithium; boron trifluoride diethyl etherate; ethylmagnesium bromide; hydrogen; silver nitrate; copper(l) chloride;
Lindlar's catalyst;
In
methanol; ethanol;
DOI:10.1016/0957-4166(95)00169-P
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) BuLi, 2.) borontrifluoride etherate / 1.) THF, hexane, -60 deg C, 15 min, 2.) THF, -70 deg C, 30 min
2: 62 percent / H2 / Lindlar catalyst / methanol / 1 h
3: 73 percent / pyridine / 24 h / 0 °C
With
pyridine; n-butyllithium; boron trifluoride diethyl etherate; hydrogen;
Lindlar's catalyst;
In
methanol;
DOI:10.1016/0957-4166(95)00169-P