1-(4-Tolyl)-4-penten-1-oxyl radical

Base Information

Chemical Name:1-(4-Tolyl)-4-penten-1-oxyl radical
CAS No.:182144-33-8
Molecular Formula:C₁₂H₁₅O
Molecular Weight:175.251
Hs Code.:

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Chemical Property of 1-(4-Tolyl)-4-penten-1-oxyl radical

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Technology Process of 1-(4-Tolyl)-4-penten-1-oxyl radical

There total 4 articles about 1-(4-Tolyl)-4-penten-1-oxyl radical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 182143-96-0
1-(1-p-Tolyl-pent-4-enyloxy)-1H-pyridine-2-thione

: 182144-33-8
1-(4-Tolyl)-4-penten-1-oxyl radical

Guidance literature:: With tri-n-butyl-tin hydride; In benzene; at 30 ℃; for 0.0166667h; Irradiation;

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 182144-33-8
1-(4-Tolyl)-4-penten-1-oxyl radical

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / tetrahydrofuran

2: CCl₄, PPh₃ / 77 °C

3: 42 percent / dimethylformamide / 1.) 0 deg C, 1 h, 2.) 25 deg C, 14 h

4: tri-n-butyltin hydride / benzene / 0.02 h / 30 °C / Irradiation

With tetrachloromethane; tri-n-butyl-tin hydride; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; benzene;

Reference yield:

: 125997-12-8
1-(4-Methylphenyl)-4-penten-1-ol

: 182144-33-8
1-(4-Tolyl)-4-penten-1-oxyl radical

Guidance literature:: Multi-step reaction with 3 steps

1: CCl₄, PPh₃ / 77 °C

2: 42 percent / dimethylformamide / 1.) 0 deg C, 1 h, 2.) 25 deg C, 14 h

3: tri-n-butyltin hydride / benzene / 0.02 h / 30 °C / Irradiation

With tetrachloromethane; tri-n-butyl-tin hydride; triphenylphosphine; In N,N-dimethyl-formamide; benzene;