C₁₈⁽¹³⁾C₂H₂₃O₇P

Base Information

Chemical Name:C₁₈⁽¹³⁾C₂H₂₃O₇P
CAS No.:1352038-51-7
Molecular Formula:C₂₀H₂₃O₇P
Molecular Weight:408.35
Hs Code.:

C<sub>18</sub><sup>(13)</sup>C<sub>2</sub>H<sub>23</sub>O<sub>7</sub>P

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈⁽¹³⁾C₂H₂₃O₇P

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Technology Process of C₁₈⁽¹³⁾C₂H₂₃O₇P

There total 3 articles about C₁₈⁽¹³⁾C₂H₂₃O₇P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 1066-50-8
Ethylphosphonic dichloride

: 1352038-50-6
C₈⁽¹³⁾CH₁₀O₃

: 1352038-51-7
C₁₈⁽¹³⁾C₂H₂₃O₇P

Guidance literature:: C₈⁽¹³⁾CH₁₀O₃; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃;

Ethylphosphonic dichloride; In tetrahydrofuran; mineral oil; at 0 ℃;
DOI:10.1039/c1cc15295e

Reference yield:

: 1352038-49-3
C₉⁽¹³⁾CH₁₂O₃

: 1352038-51-7
C₁₈⁽¹³⁾C₂H₂₃O₇P

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium iodide diethyletherate / diethyl ether; toluene / 60 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C

2.2: 0 °C

With magnesium iodide diethyletherate; sodium hydride; In tetrahydrofuran; diethyl ether; toluene; mineral oil;
DOI:10.1039/c1cc15295e

Reference yield:

: 38064-90-3
2,4-dimethoxytoluene

: 1352038-51-7
C₁₈⁽¹³⁾C₂H₂₃O₇P

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / diethyl ether; hexane / 2 h

1.2: 2 h

2.1: magnesium iodide diethyletherate / diethyl ether; toluene / 60 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C

3.2: 0 °C

With n-butyllithium; magnesium iodide diethyletherate; sodium hydride; In tetrahydrofuran; diethyl ether; hexane; toluene; mineral oil;
DOI:10.1039/c1cc15295e