benzyl 3-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranoside

Base Information

• Chemical Name: benzyl 3-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranoside
• CAS No.: 105677-96-1
• Molecular Formula: C₉₀H₉₄O₁₇
• Molecular Weight: 1447.73

Synonyms:

Chemical Property of benzyl 3-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranoside

Chemical Property:

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Useful:

Technology Process of benzyl 3-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranoside

There total 2 articles about benzyl 3-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl chloride (65827-59-0) + benzyl 2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-D-galactopyranoside (105677-95-0) → benzyl 3-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-D-galactopyranoside (105677-96-1,105761-55-5)

Guidance literature:

With mercury(II) cyanide; In acetonitrile; at 20 ℃; for 60h;

DOI:10.1016/0008-6215(87)84009-0

Reference yield: 56.1%

2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl chloride (65827-59-0) + benzyl 2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranosyl (105677-94-9) → benzyl 3-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranoside (105677-96-1,105761-55-5)

Guidance literature:

With mercury(II) cyanide; In acetonitrile; at 20 ℃; for 60h;

DOI:10.1016/0008-6215(87)84009-0

Reference yield: 82.4%

benzyl 3-O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-D-galactopyranoside (105677-96-1,105761-55-5) → benzyl 2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-3-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-β-D-galactopyranoside (105677-97-2,105814-38-8)

Guidance literature:

With pyridine; sodium methylate; In methanol; at 20 ℃; for 16h;

DOI:10.1016/0008-6215(87)84009-0

upstream raw materials:

2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl chloride

benzyl 2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-β-D-galactopyranoside

benzyl 2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-β-D-galactopyranosyl

Downstream raw materials:

benzyl 2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-3-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-β-D-galactopyranoside

benzyl 2,6-di-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-3-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-β-D-galactopyranoside

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