C₅₆H₅₇F₆NOP₂Pd

Base Information

Chemical Name:C₅₆H₅₇F₆NOP₂Pd
CAS No.:1624290-41-0
Molecular Formula:C₅₆H₅₇F₆NOP₂Pd
Molecular Weight:1042.43
Hs Code.:

C<sub>56</sub>H<sub>57</sub>F<sub>6</sub>NOP<sub>2</sub>Pd

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₆H₅₇F₆NOP₂Pd

Chemical Property:

Purity/Quality:

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Technology Process of C₅₆H₅₇F₆NOP₂Pd

There total 8 articles about C₅₆H₅₇F₆NOP₂Pd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1624315-19-0
rac-4-bromo[2.2]paracyclophan-13-ylenebis-(4-trifluoromethylphenyl)phosphine

: 1624290-41-0,1627153-77-8
C₅₆H₅₇F₆NOP₂Pd

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butyl lithium / tetrahydrofuran; pentane / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

With tert.-butyl lithium; In tetrahydrofuran; pentane;
DOI:10.1002/ejoc.201400159

Reference yield:

: 1624290-44-3
C₃₀H₂₃F₆OP

: 1624290-41-0,1627153-77-8
C₅₆H₅₇F₆NOP₂Pd

Guidance literature:: Multi-step reaction with 5 steps

1.1: bromine; iron / dichloromethane / 20 °C

2.1: diphosphorus pentasulfide / chlorobenzene / 19 h / 90 °C / Inert atmosphere

3.1: triethyl phosphite / 4 h / 130 °C / Inert atmosphere

4.1: tert.-butyl lithium / tetrahydrofuran; pentane / -78 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

5.1: tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

With diphosphorus pentasulfide; bromine; tert.-butyl lithium; iron; triethyl phosphite; In tetrahydrofuran; dichloromethane; chlorobenzene; pentane;
DOI:10.1002/ejoc.201400159

Reference yield:

: 13685-24-0
bis(4-trifluoromethylphenyl)phosphine chloride

: 1624290-41-0,1627153-77-8
C₅₆H₅₇F₆NOP₂Pd

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: bromine; iron / dichloromethane / 20 °C

3.1: diphosphorus pentasulfide / chlorobenzene / 19 h / 90 °C / Inert atmosphere

4.1: triethyl phosphite / 4 h / 130 °C / Inert atmosphere

5.1: tert.-butyl lithium / tetrahydrofuran; pentane / -78 °C / Inert atmosphere

5.2: -78 - 20 °C / Inert atmosphere

6.1: tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

With diphosphorus pentasulfide; n-butyllithium; bromine; tert.-butyl lithium; iron; triethyl phosphite; In tetrahydrofuran; hexane; dichloromethane; chlorobenzene; pentane;
DOI:10.1002/ejoc.201400159