benzhydryl (6R,7R,Z)-7-(2-(methoxyimino)-2-(2-(2-(2-(tritylamino)acetamido)acetamido)thiazol-4-yl)acetamido)-3-(((4-nitrophenoxy)carbonyloxy)methyl)-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylate

Base Information

Chemical Name:benzhydryl (6R,7R,Z)-7-(2-(methoxyimino)-2-(2-(2-(2-(tritylamino)acetamido)acetamido)thiazol-4-yl)acetamido)-3-(((4-nitrophenoxy)carbonyloxy)methyl)-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylate
CAS No.:1374584-90-3
Molecular Formula:C₅₇H₄₈N₈O₁₂S₂
Molecular Weight:1101.19
Hs Code.:

benzhydryl (6R,7R,Z)-7-(2-(methoxyimino)-2-(2-(2-(2-(tritylamino)acetamido)acetamido)thiazol-4-yl)acetamido)-3-(((4-nitrophenoxy)carbonyloxy)methyl)-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylate

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Chemical Property of benzhydryl (6R,7R,Z)-7-(2-(methoxyimino)-2-(2-(2-(2-(tritylamino)acetamido)acetamido)thiazol-4-yl)acetamido)-3-(((4-nitrophenoxy)carbonyloxy)methyl)-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylate

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Technology Process of benzhydryl (6R,7R,Z)-7-(2-(methoxyimino)-2-(2-(2-(2-(tritylamino)acetamido)acetamido)thiazol-4-yl)acetamido)-3-(((4-nitrophenoxy)carbonyloxy)methyl)-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylate

There total 3 articles about benzhydryl (6R,7R,Z)-7-(2-(methoxyimino)-2-(2-(2-(2-(tritylamino)acetamido)acetamido)thiazol-4-yl)acetamido)-3-(((4-nitrophenoxy)carbonyloxy)methyl)-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₈N₆O₇S₂

: 1374584-90-3
benzhydryl (6R,7R,Z)-7-(2-(methoxyimino)-2-(2-(2-(2-(tritylamino)acetamido)acetamido)thiazol-4-yl)acetamido)-3-(((4-nitrophenoxy)carbonyloxy)methyl)-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 0.5 h / pH 3 / Inert atmosphere

2: ethyl acetate / 1 h / Inert atmosphere

3: pyridine / dichloromethane / 2 h / 20 °C / Inert atmosphere

With pyridine; In dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1002/anie.201107810

Reference yield:

: 908093-98-1
diazodiphenylmethane

: 1374584-90-3
benzhydryl (6R,7R,Z)-7-(2-(methoxyimino)-2-(2-(2-(2-(tritylamino)acetamido)acetamido)thiazol-4-yl)acetamido)-3-(((4-nitrophenoxy)carbonyloxy)methyl)-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 0.5 h / pH 3 / Inert atmosphere

2: ethyl acetate / 1 h / Inert atmosphere

3: pyridine / dichloromethane / 2 h / 20 °C / Inert atmosphere

With pyridine; In dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1002/anie.201107810

Reference yield:

: 3397-28-2
tritylglycine N-hydroxysuccimide ester

: C₂₉H₂₈N₆O₇S₂

: 1374584-90-3
benzhydryl (6R,7R,Z)-7-(2-(methoxyimino)-2-(2-(2-(2-(tritylamino)acetamido)acetamido)thiazol-4-yl)acetamido)-3-(((4-nitrophenoxy)carbonyloxy)methyl)-8-oxo-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: ethyl acetate / 1 h / Inert atmosphere

2: pyridine / dichloromethane / 2 h / 20 °C / Inert atmosphere

With pyridine; In dichloromethane; ethyl acetate;
DOI:10.1002/anie.201107810