Carbamic acid, [6-amino-4-[[2-(hydroxyimino)-1-methyl-2-(3-nitrophenyl)ethyl]amino]-5- nitro-2-pyridinyl]-, ethyl ester

Base Information

Chemical Name:Carbamic acid, [6-amino-4-[[2-(hydroxyimino)-1-methyl-2-(3-nitrophenyl)ethyl]amino]-5- nitro-2-pyridinyl]-, ethyl ester
CAS No.:135696-25-2
Molecular Formula:C17H19N7O7
Molecular Weight:433.381
Hs Code.:
Mol file:135696-25-2.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, [6-amino-4-[[2-(hydroxyimino)-1-methyl-2-(3-nitrophenyl)ethyl]amino]-5- nitro-2-pyridinyl]-, ethyl ester

Chemical Property:

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Technology Process of Carbamic acid, [6-amino-4-[[2-(hydroxyimino)-1-methyl-2-(3-nitrophenyl)ethyl]amino]-5- nitro-2-pyridinyl]-, ethyl ester

There total 2 articles about Carbamic acid, [6-amino-4-[[2-(hydroxyimino)-1-methyl-2-(3-nitrophenyl)ethyl]amino]-5- nitro-2-pyridinyl]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 135696-13-8
2-amino-3'-nitropropiophenone oxime

: 6506-86-1
ethyl (6-amino-4-chloro-5-nitropyridin-2-yl)carbamate

: 135696-25-2
ethyl <6-amino-4-<<2-(3-nitrophenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

Guidance literature:: With triethylamine; In isopropyl alcohol; for 23h; Heating;
DOI:10.1021/jm00115a005

Reference yield:

: 135696-58-1
3'-nitro-2-phthalimidopropiophenone oxime

: 135696-25-2
ethyl <6-amino-4-<<2-(3-nitrophenyl)-1-methyl-2-oxoethyl>amino>-5-nitropyridin-2-yl>carbamate oxime

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / ethanol / 21 h / 40 °C

2: 68 percent / triethylamine / propan-2-ol / 23 h / Heating

With triethylamine; hydrazine; In ethanol; isopropyl alcohol;
DOI:10.1021/jm00115a005