[Ni2(2-[N-benzyl-N-(2-pyridylmethyl)aminomethyl]-4-methyl-6-[N-(2-pyridylmethyl)-N-(5-methyl-3-formyl-2-hydroxyphenylmethyl)aminomethyl]phenolate)(μ-OAc)2(H2O)]BPh4

Base Information

• Chemical Name: [Ni2(2-[N-benzyl-N-(2-pyridylmethyl)aminomethyl]-4-methyl-6-[N-(2-pyridylmethyl)-N-(5-methyl-3-formyl-2-hydroxyphenylmethyl)aminomethyl]phenolate)(μ-OAc)2(H2O)]BPh4
• CAS No.: 1231670-90-8
• Molecular Formula: C₂₄H₂₀B*C₄₁H₄₅N₄Ni₂O₈
• Molecular Weight: 1158.44
• Mol file: 1231670-90-8.mol

Synonyms:

Chemical Property of [Ni2(2-[N-benzyl-N-(2-pyridylmethyl)aminomethyl]-4-methyl-6-[N-(2-pyridylmethyl)-N-(5-methyl-3-formyl-2-hydroxyphenylmethyl)aminomethyl]phenolate)(μ-OAc)2(H2O)]BPh4

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Ni2(2-[N-benzyl-N-(2-pyridylmethyl)aminomethyl]-4-methyl-6-[N-(2-pyridylmethyl)-N-(5-methyl-3-formyl-2-hydroxyphenylmethyl)aminomethyl]phenolate)(μ-OAc)2(H2O)]BPh4

There total 1 articles about [Ni2(2-[N-benzyl-N-(2-pyridylmethyl)aminomethyl]-4-methyl-6-[N-(2-pyridylmethyl)-N-(5-methyl-3-formyl-2-hydroxyphenylmethyl)aminomethyl]phenolate)(μ-OAc)2(H2O)]BPh4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

nickel(II) perchlorate hexahydrate + 2-[N-benzyl-N-(2-pyridylmethyl)aminomethyl]-4-methyl-6-[N-(2-pyridylmethyl)-N-(5-methyl-3-formyl-2-hydroxyphenylmethyl)aminomethyl]phenol (1231670-94-2) + sodium tetraphenyl borate (143-66-8) + sodium acetate trihydrate (6131-90-4) → [Ni2(2-[N-benzyl-N-(2-pyridylmethyl)aminomethyl]-4-methyl-6-[N-(2-pyridylmethyl)-N-(5-methyl-3-formyl-2-hydroxyphenylmethyl)aminomethyl]phenolate)(μ-OAc)2(H2O)]BPh4 (1231670-90-8,1384168-69-7)

Guidance literature:

In methanol; mixt. of Ni salt and ligand in MeOH heated at 60°C for 15 min, acetate added, NaBPh4 added; solid filtered off, dried under vac. for 24 h; elem. anal.;

DOI:10.1021/ic300018t

upstream raw materials:

2-[N-benzyl-N-(2-pyridylmethyl)aminomethyl]-4-methyl-6-[N-(2-pyridylmethyl)-N-(5-methyl-3-formyl-2-hydroxyphenylmethyl)aminomethyl]phenol

sodium tetraphenyl borate

sodium acetate trihydrate