Technology Process of (1E,5E)-cyclonona-1,5-dien-1-yl benzoate
There total 3 articles about (1E,5E)-cyclonona-1,5-dien-1-yl benzoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: Porcine pancreatic lipase type II / 1 h / 30 °C / pH 6.9 / Enzymatic reaction
2.1: potassium hydride / 1,2-dimethoxyethane / 0 - 20 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
With
Porcine pancreatic lipase type II; potassium hydride;
In
1,2-dimethoxyethane;
DOI:10.1021/ja1092375
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrahydrofuran / 0 - 50 °C / Inert atmosphere
2.1: potassium hydride / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere
3.1: potassium hydride / 1,2-dimethoxyethane / 0 - 20 °C / Inert atmosphere
3.2: 0 - 20 °C / Inert atmosphere
With
potassium hydride;
In
tetrahydrofuran; 1,2-dimethoxyethane; N,N-dimethyl-formamide;
2.1: ring-enlarging anionic oxy-Cope rearrangement;
DOI:10.1021/ja1092375
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydride / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere
2.1: potassium hydride / 1,2-dimethoxyethane / 0 - 20 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
With
potassium hydride;
In
1,2-dimethoxyethane; N,N-dimethyl-formamide;
1.1: ring-enlarging anionic oxy-Cope rearrangement;
DOI:10.1021/ja1092375
