C₂₂H₂₇BrN₄O₄

Base Information

Chemical Name:C₂₂H₂₇BrN₄O₄
CAS No.:1319191-69-9
Molecular Formula:C₂₂H₂₇BrN₄O₄
Molecular Weight:491.385
Hs Code.:

C<sub>22</sub>H<sub>27</sub>BrN<sub>4</sub>O<sub>4</sub>

Synonyms:

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Chemical Property of C₂₂H₂₇BrN₄O₄

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Technology Process of C₂₂H₂₇BrN₄O₄

There total 4 articles about C₂₂H₂₇BrN₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1319191-60-0
C₁₉H₂₄BrN₃O₄

: 1319191-69-9
C₂₂H₂₇BrN₄O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C

1.2: 20 °C

2.1: diisobutylaluminium hydride / dichloromethane; hexane / 5 h / -78 °C

2.2: 0.25 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C

3.2: 15 h / 20 °C

4.1: hydrogenchloride / 1,4-dioxane / 5 h / 50 °C

5.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 1.33 h / 20 °C

With hydrogenchloride; sodium hydride; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; HATU; In 1,4-dioxane; hexane; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1319191-61-1
C₂₅H₃₈BrN₃O₅Si

: 1319191-69-9
C₂₂H₂₇BrN₄O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / dichloromethane; hexane / 5 h / -78 °C

1.2: 0.25 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C

2.2: 15 h / 20 °C

3.1: hydrogenchloride / 1,4-dioxane / 5 h / 50 °C

4.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 1.33 h / 20 °C

With hydrogenchloride; sodium hydride; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; HATU; In 1,4-dioxane; hexane; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1319191-63-3
C₂₃H₃₆BrN₃O₄Si

: 1319191-69-9
C₂₂H₂₇BrN₄O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C

1.2: 15 h / 20 °C

2.1: hydrogenchloride / 1,4-dioxane / 5 h / 50 °C

3.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 1.33 h / 20 °C

With hydrogenchloride; sodium hydride; N-ethyl-N,N-diisopropylamine; HATU; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; mineral oil;