C₂₈H₄₁N₇O₉

Base Information

Chemical Name:C₂₈H₄₁N₇O₉
CAS No.:1360566-63-7
Molecular Formula:C₂₈H₄₁N₇O₉
Molecular Weight:619.675
Hs Code.:

C<sub>28</sub>H<sub>41</sub>N<sub>7</sub>O<sub>9</sub>

Synonyms:

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Chemical Property of C₂₈H₄₁N₇O₉

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Technology Process of C₂₈H₄₁N₇O₉

There total 11 articles about C₂₈H₄₁N₇O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1221741-69-0
C₂₄H₄₂N₂O₅Si

: 1360566-63-7
C₂₈H₄₁N₇O₉

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium carbonate / tetrahydrofuran; water / 0.17 h / 0 °C

2.1: hydrogenchloride; titanium(III) chloride; sodium acetate; zinc / methanol; dichloromethane; water / 24 h / -50 °C / Inert atmosphere

3.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

4.1: monochloromethanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

6.1: 20 % Pd(OH)2/C; hydrogen / methanol / 3 h / 20 °C

7.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 2 h / 20 °C

8.1: pyridine / 3 h / 20 - 50 °C

9.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 5 h / 20 °C

10.1: dichloromethane / 1 h / 0 °C / Inert atmosphere

10.2: 3 h / 0 - 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; titanium(III) chloride; monochloromethanesulfonyl chloride; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; sodium acetate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; mercury dichloride; zinc; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201101058

Reference yield:

: 1360566-51-3
C₂₄H₄₀N₂O₆Si

: 1360566-63-7
C₂₈H₄₁N₇O₉

Guidance literature:: Multi-step reaction with 11 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1 h / -40 °C

1.2: 5 h / -40 - 0 °C

2.1: potassium carbonate / tetrahydrofuran; water / 0.17 h / 0 °C

3.1: hydrogenchloride; titanium(III) chloride; sodium acetate; zinc / methanol; dichloromethane; water / 24 h / -50 °C / Inert atmosphere

4.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

5.1: monochloromethanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

7.1: 20 % Pd(OH)2/C; hydrogen / methanol / 3 h / 20 °C

8.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 2 h / 20 °C

9.1: pyridine / 3 h / 20 - 50 °C

10.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 5 h / 20 °C

11.1: dichloromethane / 1 h / 0 °C / Inert atmosphere

11.2: 3 h / 0 - 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; titanium(III) chloride; monochloromethanesulfonyl chloride; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; sodium acetate; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; mercury dichloride; zinc; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201101058

Reference yield:

: 1221741-71-4
C₃₂H₄₈N₂O₇Si

: 1360566-63-7
C₂₈H₄₁N₇O₉

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogenchloride; titanium(III) chloride; sodium acetate; zinc / methanol; dichloromethane; water / 24 h / -50 °C / Inert atmosphere

2.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

3.1: monochloromethanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

5.1: 20 % Pd(OH)2/C; hydrogen / methanol / 3 h / 20 °C

6.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 2 h / 20 °C

7.1: pyridine / 3 h / 20 - 50 °C

8.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 5 h / 20 °C

9.1: dichloromethane / 1 h / 0 °C / Inert atmosphere

9.2: 3 h / 0 - 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; titanium(III) chloride; monochloromethanesulfonyl chloride; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; sodium acetate; triethylamine; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; mercury dichloride; zinc; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201101058