C₂₃H₂₅NOS

Base Information

Chemical Name:C₂₃H₂₅NOS
CAS No.:1428366-36-2
Molecular Formula:C₂₃H₂₅NOS
Molecular Weight:363.524
Hs Code.:

Synonyms:

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Chemical Property of C₂₃H₂₅NOS

Chemical Property:

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Technology Process of C₂₃H₂₅NOS

There total 5 articles about C₂₃H₂₅NOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428366-12-4
C₁₅H₂₇NOSSi

: 1428366-36-2
C₂₃H₂₅NOS

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2: titanium(IV) tetraethanolate / dichloromethane / Inert atmosphere; Reflux

3: toluene / 20 °C / Inert atmosphere

With titanium(IV) tetraethanolate; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo400354r

Reference yield:

: 1428365-94-9
(R_s)-2-phenylpropyl-2-sulfinamide

: 1428366-36-2
C₂₃H₂₅NOS

Guidance literature:: Multi-step reaction with 2 steps

1: titanium(IV) tetraethanolate / dichloromethane / Inert atmosphere; Reflux

2: toluene / 20 °C / Inert atmosphere

With titanium(IV) tetraethanolate; In dichloromethane; toluene;
DOI:10.1021/jo400354r

Reference yield:

: 16325-88-5
α,α-dimethylbenzylmercaptan

: 1428366-36-2
C₂₃H₂₅NOS

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium iodide; dihydrogen peroxide / ethyl acetate; water / 18 h / 20 °C

2.1: dihydrogen peroxide; (1S,2R)-1-(3,5-di-tert-butyl-2-hydroxybenzylideneamino)-2,3-dihydro-1H-inden-2-ol; bis(acetylacetonate)oxovanadium / water; acetone / 46 h / 0 °C

3.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

5.1: titanium(IV) tetraethanolate / dichloromethane / Inert atmosphere; Reflux

6.1: toluene / 20 °C / Inert atmosphere

With titanium(IV) tetraethanolate; n-butyllithium; bis(acetylacetonate)oxovanadium; (1S,2R)-1-(3,5-di-tert-butyl-2-hydroxybenzylideneamino)-2,3-dihydro-1H-inden-2-ol; tetrabutyl ammonium fluoride; dihydrogen peroxide; sodium iodide; In tetrahydrofuran; dichloromethane; water; ethyl acetate; acetone; toluene;
DOI:10.1021/jo400354r